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用超临界CO2脱除绿茶浓缩液中咖啡碱的工艺研究 总被引:3,自引:0,他引:3
对绿茶浓缩液中咖啡碱的超临界CO2萃取工艺进行了研究,通过4因素正交试验探讨了浓缩液的浓度、操作压强、操作温度、萃取时间对咖啡碱脱除率的影响。结果表明,超临界CO2萃取技术可以有效地脱除绿茶浓缩液中大部分的咖啡碱,在此基础上完成了用超临界CO2脱除绿茶浓缩液中咖啡碱的连续作业试验,从而获得了加工脱咖啡碱绿茶浓缩液或速溶绿茶的新工艺。 相似文献
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为了对比冷榨法、溶剂浸出法、超临界CO2萃取法3种提取方法所得紫斑牡丹籽油的品质,以甘肃紫斑牡丹籽为研究对象,从外观品质、出油率、理化特性及抗氧化能力方对3种方法提取的牡丹籽油品质进行观测。结果表明,采用溶剂浸提法提取的牡丹籽油得率最高,为27.27%;其次是超临界CO2萃取法,为22.80%;冷榨法最低,为20.17%。采用超临界CO2萃取法提取的牡丹籽油酸值和过氧化值低,抗氧化性能强,油品质量最高。采用冷榨法提取的牡丹籽油酸值低,品质较好,方法操作简单。3种提取方法各有特点,生产中可根据具体需求选择适用。 相似文献
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为了研究超临界CO2作为非水相介质在生化反应工程中的作用,有必要考察超临界CO2处理对微生物活性的影响。本文以乳酸杆菌为试验菌种,进行了该菌在不同参数超临界CO2处理对菌体生长曲线、耐渗透压能力、耐酸能力、抑菌能力、降解胆固醇能力等活性指标影响的研究。结果表明:当提高超临界CO2压强或延长超临界CO2处理时间,乳酸杆菌的活性指标会发生如下变化:生长曲线的最大菌体浓度降低,但菌体的生长速率差异不大;菌体的耐渗透能力、耐酸能力降低;所得的抑菌圈比较明显,但抑菌圈直径减小;平均胆固醇降解率降低,而且长时间处理对降解效果的影响比高压强处理的明显。因此,在工程应用中需要研究一定的弥补措施。 相似文献
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CO2 efflux plays a key role in carbon exchange between the biosphere and atmosphere, but our understanding of the mechanism controlling its temporal and spatial variations is limited. The purpose of this study is to determine annual soil CO2 flux and assess its variations in arable subtropical soils of China in relation to soil temperature, moisture, rainfall, microbial biomass carbon (MBC) and dissolved organic carbon (DOC) using the closed chamber method. Soils were derived from three parent materials including granite (G), tertiary red sandstone (T) and quaternary red clay (Q). The experiment was conducted at the Ecological Station of Red Soil, The Chinese Academy of Sciences, in a subtropical region of China. The results showed that soil CO2 flux had clear seasonal fluctuations with the maximum value in summer, the minimum in winter and intermediate in spring and autumn. Further, significant differences in soil CO2 flux were found among the three red soils, generally in the order of G>T>Q. The average annual fluxes were estimated as 2.84, 2.13 and 1.41 kg CO2 m−2 year−1 for red soils derived from G, T and Q, respectively. Soil temperature strongly affects the seasonal variability of soil CO2 flux (85.0-88.5% of the variability), followed by DOC (55.8-84.4%) and rainfall (43.0-55.8%). The differences in soil CO2 flux among the three red soils were partly explained by MBC (33.7-58.9% of the variability) and DOC (23.8-33.6%). 相似文献
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Y. Kuzyakov 《Soil biology & biochemistry》2006,38(3):425-448
Five main biogenic sources of CO2 efflux from soils have been distinguished and described according to their turnover rates and the mean residence time of carbon. They are root respiration, rhizomicrobial respiration, decomposition of plant residues, the priming effect induced by root exudation or by addition of plant residues, and basal respiration by microbial decomposition of soil organic matter (SOM). These sources can be grouped in several combinations to summarize CO2 efflux from the soil including: root-derived CO2, plant-derived CO2, SOM-derived CO2, rhizosphere respiration, heterotrophic microbial respiration (respiration by heterotrophs), and respiration by autotrophs. These distinctions are important because without separation of SOM-derived CO2 from plant-derived CO2, measurements of total soil respiration have very limited value for evaluation of the soil as a source or sink of atmospheric CO2 and for interpreting the sources of CO2 and the fate of carbon within soils and ecosystems. Additionally, the processes linked to the five sources of CO2 efflux from soil have various responses to environmental variables and consequently to global warming. This review describes the basic principles and assumptions of the following methods which allow SOM-derived and root-derived CO2 efflux to be separated under laboratory and field conditions: root exclusion techniques, shading and clipping, tree girdling, regression, component integration, excised roots and insitu root respiration; continuous and pulse labeling, 13C natural abundance and FACE, and radiocarbon dating and bomb-14C. A short sections cover the separation of the respiration of autotrophs and that of heterotrophs, i.e. the separation of actual root respiration from microbial respiration, as well as methods allowing the amount of CO2 evolved by decomposition of plant residues and by priming effects to be estimated. All these methods have been evaluated according to their inherent disturbance of the ecosystem and C fluxes, and their versatility under various conditions. The shortfalls of existing approaches and the need for further development and standardization of methods are highlighted. 相似文献
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M. Maier H. Schack-KirchnerE.E. Hildebrand D. Schindler 《Agricultural and Forest Meteorology》2011,151(12):1723-1730
In the long term, all CO2 produced in the soil must be emitted by the surface and soil CO2 efflux (FCO2) must correspond to soil respiration (Rsoil). In the short term, however, the efflux can deviate from the instantaneous soil respiration, if the amount of CO2 stored in the soil pore-space (SCO2) is changing. We measured FCO2 continuously for one year using an automated chamber system. Simultaneously, vertical soil profiles of CO2 concentration, moisture, and temperature were measured in order to assess the changes in the amount of CO2 stored in the soil. Rsoil was calculated as the sum of the rate of change of the CO2 storage over time and FCO2. The experiment was split into a warm and a cold season. The dependency of soil respiration and soil efflux on soil temperature and on soil moisture was analyzed separately. Only the moisture-driven model of the warm season was significantly different for FCO2 and Rsoil. At our site, a moisture-driven soil-respiration model derived from CO2 efflux data would underestimate the importance of soil moisture. This effect can be attributed to a temporary storage of CO2 in the soil pore-space after rainfalls where up to 40% of the respired CO2 were stored. 相似文献