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991.
香菇多糖提取纯化研究 总被引:8,自引:0,他引:8
用0.2mol/L三氯乙酸、0.2mol/L氢氧化钠、1.0mol/L乙酸、蒸馏水为提取溶剂,结合超声波处理等方法从香菇子实体中提取香菇多糖,提取液经甲醇除杂、沉淀处理得粗多糖。粗多糖用CTAB络合沉淀,沉淀物乙酸溶解后取上清再用甲醇沉淀,沉淀物冻干得纯化多糖。分析检测结果显示干香菇三氯乙酸提取的纯化多糖的含量高达93.1%、提取得率达0.324%。薄层分析表明,纯化香菇多糖由葡萄糖、甘露糖、半乳糖、木糖组成。纯化多糖用Sephadex G-100凝胶层析,洗脱液经苯酚-硫酸法检测为单一吸收峰,红外光谱显示其具有多糖类的特征吸收峰。 相似文献
992.
酸催化下苯酚液化木材的制备与表征 总被引:19,自引:3,他引:19
在硫酸作用下用苯酚对人工林杨木和杉木进行液化,考察反应时间、反应温度等对液化反应的影响,并对液化产物进行表征分析.结果表明:1)在硫酸催化下,杨木和杉木被苯酚液化的历程相似,但残渣含量稍有不同.酸性催化剂不仅对纤维素和半纤维素起作用,对木质素也起作用.2)反应温度比反应时间对液化效率的影响大,二者均能影响液化产物的分子量和分子量分布.通常杉木液化产物的重均分子量高于杨木.3)液化过程中,木质素和半纤维素首先被液化,最后是纤维素.木材组分的分解、酚化和再缩聚反应主宰整个液化动力学过程及液化产物的结构特征. 相似文献
993.
Jie Liu Rumi Fujita Michiko Sato Kuniyoshi Shimizu Fumiko Konishi Kiyoshi Noda Shoichiro Kumamoto Chie Ueda Hisatoshi Tajiri Shuhei Kaneko Yoshitaro Suimi Ryuichiro Kondo 《Journal of Wood Science》2005,51(2):189-192
The inhibitory effects of 102 methanol extracts of 40 mycelia, 9 culture fluids, and 53 fruiting bodies of 40 strains of Ganoderma lucidum on 5-reductase were investigated. The methanol extract of the fruiting body of each strain was found to show the strongest 5-reductase inhibitory activity among the extracts tested. 相似文献
994.
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996.
主要综述了季铵盐类化合物(QAC)在用作木材防腐剂时的耐腐性、抗流失性及其与木材的结合机理等方面的研究概况,分析了实验室耐腐性和野外实验耐腐性结果不一致的原因。此外也介绍了对季铵盐进行改性处理方面的一些研究进展。 相似文献
997.
Mathieu Fortin Gaétan Daigle Chhun-Huor Ung Jean Bégin Louis Archambault 《European Journal of Forest Research》2007,126(4):573-585
This study proposes a within-subject variance-covariance (VC) structure to take into account repeated measurements and heteroscedasticity
in a context of growth modeling. The VC structure integrates a variance function and a continuous autoregressive covariance
structure. It was tested on a nonlinear growth model parameterized with data from permanent sample plots. Using a stand-level
approach, basal area growth was independently modeled for red spruce (Picea rubens Sarg.) and balsam fir [Abies balsamea (L.) Mill.] in mixed stands. For both species, the implementation of the VC structure significantly improved the maximum
likelihood of the model. In both cases, it efficiently accounted for heteroscedasticity and autocorrelation, since the normalized
residuals no longer exhibited departures from the assumptions of independent error terms with homogeneous variances. Moreover,
compared with traditional nonlinear least squares (NLS) models, models parameterized with this VC structure may generate more
accurate predictions when prior information is available. This case study demonstrates that the implementation of a VC structure
may provide parameter estimates that are consistent with asymptotically unbiased variances in a context of nonlinear growth
modeling using a stand-level approach. Since the variances are no longer biased, the hypothesis tests performed on the estimates
are valid when the number of observations is large. 相似文献
998.
Cao Jin-zhen Yu Li-li You Xiao-di Kamdem D. Pascal 《中国林学(英文版)》2007,9(4):239-245
In order to clarify the interaction between copper and wood substances in wood treated with copper containing water-borne wood preservatives, the dielectric constant ε′ and dielectric loss factor ε″ of untreated wood and wood treated with four concentration levels of copper-ethanolamine (Cu-EA) solutions were determined within a temperature range from –100 to 40°C and a frequency range from 100 to 1 MHz. Three dielectric relaxation processes were observed in the ε″ spectrum; among them R-I is based on the reorientation of methylol groups in the amorphous region of wood cell walls and R-II is related to wood extractives. R-III appeared in Cu-EA treated wood, and its magnitude decreases with the concentration of Cu-EA solutions used in this experiment. This relaxation process was considered to be based on the reorientation of copper-ethanolamine-wood complexes in wood cell walls. At low copper retention, the hydrogen in the complex can form hydrogen bonding with adjacent hydroxyl groups, which results in a strong bonding state between copper and wood; at high copper retention, the numerous copper-ethanolamine complexes not only hinder them from forming hydrogen bonding with adjacent wood molecules due to steric hindrance, but also weaken the interaction between wood molecules themselves, which corresponds to reducing ε″ values of both R-I and R-III processes. The results explain the fact of in-creasing copper leaching in wood treated with high concentration copper-based water-borne preservatives. 相似文献
999.
在气候干燥、寒冷的西北地区 ,引进具有耐干旱、贫瘠 ,抗寒冷 ,抗盐碱等多种优良特性的常绿或准常绿饲料灌木四翅滨藜 ,经过 2a生长全过程的栽培试验 ,观测结果表明 :在不同土壤类型下 ,新梢生长量、扦插育苗的成活率、保存率都表现出差异性。但移栽苗的成活率、保存率差异不大 ,表现出较强的适应性。而在中、强盐碱性土壤、(粗 )砂土中仍能正常生长 ,但新梢生长量低 ,分枝减少 相似文献
1000.