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噻嗪·异丙威25%可湿性粉剂的气相色谱分析
引用本文:程运斌,刘育清,顾辉,周扬,许国建.噻嗪·异丙威25%可湿性粉剂的气相色谱分析[J].农药科学与管理,2010,31(4):40-42.
作者姓名:程运斌  刘育清  顾辉  周扬  许国建
作者单位:1. 湖北省农科院农业测试与科技信息中心,湖北,武汉,430064
2. 湖北省农药检定管理所,湖北,武汉,430070
摘    要:本文介绍了以5%OV-101色谱柱固定相,邻苯二甲酸二丁酯为内标物,用FID检测器利用程序升温对噻嗪·异丙威25%可湿性粉剂2种组分的气相色谱分离测定方法。结果表明,噻嗪酮和异丙威的标准偏差分别为0.026、0.047,变异系数分别为0.32%、0.28%,噻嗪酮的回收率为99.34%~101.03%,异丙威的回收率为99.16%~101.47%。该方法简便、快捷、准确。

关 键 词:噻嗪酮  异丙威  气象色谱  分析

Analysis of buprofezin and isoprocarb 25% WP by Gas Chromatography
Cheng Yunbin,Liu Yuqing,Gu Hui,Zhou Yang,Xu Guojian.Analysis of buprofezin and isoprocarb 25% WP by Gas Chromatography[J].Pesticide Science and Administration,2010,31(4):40-42.
Authors:Cheng Yunbin  Liu Yuqing  Gu Hui  Zhou Yang  Xu Guojian
Institution:Agricultural Testing & Information Center/a>;Hubei Academy of Agricultural Sciences/a>;Wuhan 430064;Institute for the Control of Agrochemicals of Hubei Province/a>;Wuhan 430070/a>;China
Abstract:An analytical method for the determination of buprofezin, isoprocarb 25% WP by GC was described in this paper. The samples were separated in a column packed with OV-101 and detected by flame ionization detector. The results showed that the standard deviations were 0.026 and 0.047, the coefficients of variation were 0.32% and 0.28%, the average recoveries were 99.34%-101.03%% and 99.16%-101.47% for buprofezin and isoprocarb respectively. This method is convenient, rapid and accuracy.
Keywords:buprofezin  isoprocarb  GC  analysis  
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