| 钩藤中钩藤碱的提取和含量测定 |
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| 引用本文： | 潘俊,王柏人,曾启华,高智席,朱秀诗.钩藤中钩藤碱的提取和含量测定[J].安徽农业科学,2011,39(30):18523-18525. |
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| 作者姓名： | 潘俊 王柏人 曾启华 高智席 朱秀诗 |
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| 作者单位： | 1. 遵义师范学院化学系,贵州遵义,563002
2. 遵义市产品质量检验检测院,贵州遵义,563002 |
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| 摘 要： | 目的]研究钩藤中钩藤碱的提取和含量测定方法。方法]采用生物碱回流提取方法提取,采用高效液相色谱法对钩藤中钩藤碱的含量进行测定并计算提取率。结果]专属性考察结果显示,钩藤碱的保留时间约为18.843 min,异钩藤碱的保留时间约在22.323min,两峰分离度良好,且钩藤药材中其他成分不干扰测定;含量测定结果显示,钩藤碱和异钩藤碱的含量分别为23.23、129.17μg/g,加样回收试验平均回收率分别为99.12%、101.33%,RSD分别为1.84%、1.56%。结论]该方法稳定、有效、准确度高,可用于钩藤中钩藤碱的含量测定。
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| 关 键 词： | 钩藤（UNCARIAE RAMULUS CUM UNCIS） 钩藤碱 高效液相色谱法 |
Extraction and Content Determination of Rhynchophylline from UNCARIAE RAMULUS CUM UNCIS |
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| PAN Jun et al.Extraction and Content Determination of Rhynchophylline from UNCARIAE RAMULUS CUM UNCIS[J].Journal of Anhui Agricultural Sciences,2011,39(30):18523-18525. |
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| Authors: | PAN Jun |
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| Institution: | PAN Jun et al(Department of Chemistry,Zunyi Normal College,Zunyi,Guizhou 563002) |
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| Abstract: | Objective] The aim was to study on the extraction and content deter mination of rhynchophylline from UNCARIAE RAMULUS CUM UNCIS.Method] Extraction method of traditional alkaloids was adopted.And modern analysis method HPLC was used to deter mine the content of rhynchophylline.Rhynchophylline content in UNCARIAE RAMULUS CUM UNCIS was calculated.Result] Specialization investigation showed that the retention time of rhynchophylline was about 18.843 min,and that of isorhynchophylline was 22.323 min.The two p... |
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| Keywords: | UNCARIAE RAMULUS CUM UNCIS Rhynchophylline HPLC |
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