| 薄层色谱和液相色谱法鉴别中兽药散剂中掺加的磺胺喹噁啉钠 |
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| 引用本文： | 高迎春.薄层色谱和液相色谱法鉴别中兽药散剂中掺加的磺胺喹噁啉钠[J].中国兽药杂志,2010,44(2):23-25. |
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| 作者姓名： | 高迎春 |
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| 作者单位： | 山东省兽药质量检验所,济南,250022 |
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| 摘 要： | 对磺胺喹噁啉钠采用硅胶GF254板为固定相,以正丁醇-浓氨水(15∶3)为展开剂,用薄层色谱鉴别中兽药散剂中磺胺喹噁啉钠分离较好,斑点显色清晰且无干扰,可用于中药散剂中非法添加物磺胺喹噁啉钠的快速筛选。采用C18柱为固定相,以甲醇-乙腈-水-冰乙酸(2∶2∶9∶0.2)为流动相,紫外检测波长为270 nm。液相色谱鉴别中药散剂中非法添加磺胺喹噁啉钠分离良好,无干扰峰,可用于中兽药散剂中非法添加物磺胺喹噁啉钠的鉴别。
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| 关 键 词： | 薄层色谱法 液相色谱法 磺胺喹噁啉钠 |
| 收稿时间： | 2009/10/28 0:00:00 |
| 修稿时间： | 2010/1/11 0:00:00 |
Identification Sulfaqiunoxline Sodium Adding to Herb Veterinary Drug Compound Preparation by TLC and HPLC |
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| gaoyingchun.Identification Sulfaqiunoxline Sodium Adding to Herb Veterinary Drug Compound Preparation by TLC and HPLC[J].Chinese Journal of Veterinary Drug,2010,44(2):23-25. |
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| Authors: | gaoyingchun |
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| Institution: | GAO Ying-chun,SU MEI,WEI Xiu-li,WANG YAN,ZHANG Zhi-min(Sh,ong Provincial Veterinary Medicine Supervision Institute,jinan,250022) |
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| Abstract: | TLC and HPLC method were established for the determination of sulfaqiunoxline sodium in herb veterinary drug compound preparation.TLC condition： Drug was separated on silica gel thin layer chromatography plate;developing agent was n-butanol/stronger ammonia water（15∶3）.HPLC conditons： the chromatography column was C18 column of 150 mm×4.6 mm,5 μm;mobile phase was methanol-acetonitrile-water-acetic acid（2∶2∶9∶0.2,V/V）;Determination was by UV detection at 270 nm.This meathod identifying sulfaqiunoxline sodium adding to herb veterinary drug compound preparation is successfully feasible. |
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| Keywords: | TLC HPLC sulfaqiunoxline sodium |
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