Analysis on AE characteristic and its confining pressure effect of outburst coal containing gas

Briquette samples made of outburst coal are taken as study objects to study AE characteristic and its confining pressure effect by using self-developed equipment, Shimazu servo test machine and AE monitor system, and the characteristic of AE parameters are analyzed, too. The results show that in the process of outburst coal containing gas triaxial compression, there is no serious dense or sparse area of AE events, but three relative dense appear in compression phase, middle area of linear elastic stage and near peaking phase area so that the characteristic of AE events look like three peaks. But the amplitude of AE events is small and the good consistency between energy change and amplitude change is showed. Microstructure change caused by external stress field change, fracture and fragmentation of particle of samples, movement besides particle of samples and microstructure change caused by dissipation of gas are the sources of AE events. The number of AE events is reduced as the confining pressure is increased, but the influence on total number of AE events caused by confining pressure show nonlinear, expressed by quadratic function. The number of larger amplitude of AE events show decreasing tendency as the confining pressure is increased, the relation between numbers of AE events whose amplitude is more than certain value and confining pressure is expressed by quadratic function.     

The influence of initial internal structure of coal sample on gas flow characteristic

Three kinds of coal samples with different components are chosen as study objects.Density calculation and SEM are adopted to study their internal structures,and a self made triaxial gas seepage instrument is used to study their internal gas flow characteristics.The results show that internal structures of coal samples made of different particle size coal powders under identical external conditions are various,and nonlinearity is presented on the influence caused by fabric.Gas flow characteristic is complex in complete stress strain process,generally it firstly increases and then decreases,initial gas flow velocity is lower than the one after the failure of coal sample,and obvious hysteretic nature of gas flow characteristic is showed.The influence of gas flow characteristic caused by initial internal structure of coal sample is nonlinear and the stress sensitivity is high on the influence of gas flow characteristic caused by initial internal structure.The more complex the initial internal structure of the coal sample is,the lower the axial tress sensitivity is,and the higher the confining pressure sensitivity is.     

围压与含水率对小麦堆弹性模量影响的实验研究

使用应变控制式三轴仪,测定了不同围压和含水率条件下的小麦堆弹性模量,并分析了围压与含水率对小麦堆弹性模量的影响.实验结果表明：同一含水率下,小麦堆（含水率为11.88％ w.b、12.91％ w.b、14.40％ w.b、15.40％ w.b、16.85％ w.b）弹性模量随着围压（50 kPa～200 kPa）增大而增大;同一围压下,小麦堆的弹性模量随着水分的增大而减小.     

Experimental study on acoustic emission characteristics of coal rock at different confining pressure

This paper conducts experimental investigation on acoustic emission(AE) characteristics of coal rock at uniaxial and triaxial compression by MTS815 rock mechanics test system. The results show that the variation of AE has tendency effect at uniaxial compression and confining pressure experiments. We indicate that AE signal decreases significantly in the elastic stage, and the relatively quiet period of AE before the specimens failure is not obvious under confining pressure. The AE amplitude distribution with time and its envelope line can indirectly reflect the trend of stress. The AE events peak stress and elastic modulus decrease with the temperature increase, and the value of m which reflects the cumulative distribution of amplitude increases as the confining pressure rises. The results also show that the AE frequency distributes in three frequency domains, and the proportions of dominant frequency significantly increase while the specimens are broken.     

稻谷堆弹性模量的实验测定与研究

利用TSZ-6A型应变控制式三轴仪进行三轴实验,测定围压分别为50 kPa、100 kPa、150 kPa、200 kPa时,稻谷堆（水分为11.89%w.b,13.55%w.b,15.73%w.b,17.62%w.b）的弹性模量,同时研究围压和水分与稻谷堆弹性模量的关系。实验结果表明：对于水分范围为11.89%~17.62%w.b的稻谷堆,在围压为50 kPa~200kPa的范围内,其弹性模量范围为8.69 MPa~37.07 MPa。根据围压与稻谷堆弹性模量的关系可以拟合得到方程：y=Ax＋B,其中,A、B为与水分有关的参数。在相同水分条件下,稻谷堆的弹性模量随着围压的增大而增大;在相同围压条件下,稻谷堆的弹性模量与水分没有显著的相关性。     

Experimental analysis of matrix shrinkage’s influence on mechanical permeability of gas filled coal

Based on the coal seam of Zhao zhuang coal mine and Si he coal mine belong to Jin cheng anthracite Mining Group in Shanxi province, by using the self developed three axial servo controlled seepage equipment for hot fluid solid coupling of coal containing methane, parallel experiments for permeability of helium and methane under different gas pressures are carried out to quantitatively study the influence of Klinkenberg effects on the permeability of coal. Meanwhile, the problem of permeability decreasing caused by fluid pressure decreasing and gas desorption is eliminated by controlling the effective stress. The results show thatthe Klinkenberg effect is obvious under low gas pressure. With the increase of gas pressure, the permeability of coal decreases at first and then increases. The inflection points of gas pressure for Klinkenberg effect are about 0.9 MPa both for coal samples in Zhao zhuang coal mine and Si he coal mine. When the effective stress is constant, with the increase of gas pressure, the permeability increment caused by Klinkenberg effect decreases, while permeability increment caused by coal matrix shrinkage increases. Coal matrix shrinkage has a close relationship with the mechanical properties of coal rock mass. For the coal sample with a poor mechanical property, coal matrix shrinkage is more obvious.     

Experiment of the gas effect on coal mechanical properties under zero effective confirming pressure

Considering the seal and storage of gas, mechanical index of coal containing gas is usually obtained by normal three-axis experiment. While, according to national standard, mechanical index of coal is usually tested by uniaxial experiment. By utilizing the gas sealing system, an analogic uniaxial experiment method is proposed. Through designed experiments, the effect of gas on mechanical properties and mechanical response of the coal sample when effective confirming pressure is 0 is studied too. The experimental results show that pore gas changes the mechanical response of complete deformation stage, but the trend of change gradually weakens as the gas pressure increases, and it means that non-mechanical effects caused by absorbed gas play a leading role gradually.     

Test on engineering properties of unsaturated undisturbed loess Q2

A series of triaxial shear tests with controlled constant confining pressure are conducted to study the failure modes, effects of deformation, strength and yield properties of unsaturated undisturbed loess Q2, with improved SJ-1A triaxial shear equipment. The test results show that the failure mode of unsaturated undisturbed loess Q2 is shear failure with the rupture angle between 55 and 61 degree; Shear dilatancy is shown under low confining pressure, and shear shrinkage is shown under high confining pressure; The stress-strain curves of undisturbed loess Q2 will change from perfectly plastic to weak strain softening as the confining pressure increases; A effective method is suggested to identify the field stress of undisturbed loess Q2 under triaxial shear condition with the curves of - q/p ; when the confining pressure increases, the deviatoric yield stress qy has a logarithmic relationship with net mean yield stress py .     

小麦堆体变模量的测定与实验研究

利用应变控制式三轴仪对小麦的体积压缩和体变模量进行了实验测定,并探讨了围压和水分对体变模量的影响。结果表明:小麦堆的体积随着围压的增大而减小;小麦堆(水分为13.7%、16.4%、18%)的体变模量随着围压(5 kPa～30 kPa)的增大而增大,它们的体变模量的范围分别为173.5 kPa～259.3 kPa、164 kPa～240 kPa、151 kPa～229.4kPa;小麦堆体变模量随着水分的增大而减小,当小麦堆围压为30 kPa,水分为13.7%～18%时,它的体变模量变化范围为223.5 kPa～270 kPa。     

RESEARCH ON THE MECHANISM OF GAS OUTBURST INITATION IN MINES

The mechanism of coal-gas outburst iniration is comprehensively analysed. The direct courses of initating coal-gas outburst are the sudden loss of confining stresses and the gas pressure gradient in coal seam. The effects of working face's advancing rate, geological conditions and gas pressure gradient as well as mechanical & physical characteristics of coal on outburst initation are expounded by means of mathematic analyses about gas seepage which takes place in coal seams. The results are of certain practical significance and reference value to further quantitive study of outburst and its predication.     

Multi-field coupling effect on coalbed methane seepage characteristics and numerical simulation

This paper studies the seepage of coal samples under the influence of each single factor, the axial stress, confining pressure, gas pressure, and temperature by experiments. It uses Ansys12.0 to numerically simulate the law of coalbed methane seepage, coal deformation, pore pressure, the distribution of flow field under the influence of each single field and multi-field coupled. The numerical simulation show that the result of numerical simulation of gas seepage law in the coal under each single fields is basically the same as the experimental result. The curve of gas seepage and average effective stress under the condition of multi-field coupled is negative exponential relationship. Stress influenced the deformation of the specimen is greater than the seepage field. The axial stress on the deformation of the specimen is greater than confining presses The influence on the flow field by confining pressure is greater than axial stress, the influence of axial stress on the pore pressure is greater than confining pressure, pore-pressure under the action of multi-field is bigger than pro-pressure under each single field. To study the seepage law of coalbed methane, it should consider the influence of gas-solid-heat at the same time.     

Analysis of the Lateral Deformation of Structural Soft Dredger Fill with True Triaxial Test

In order to study the mechanical properties and structural properties of soft dredger fill under lateral deformation. Based on true triaxial and WF stress path apparatus, lateral unloading undrained tests were carried out. The results derived from true triaxial test, WF stress path test and routine triaxial shear test were analyzed. The contrastive conclusions are as follows: The stress-strain curve of true triaxial unloading test shows a softening behavior, which is different from the hardening behavior for that of conventional triaxial shear test. With the increase of initial confined pressure, the dilatancy of soil transfers from shrinkage to expansion. The structural yield stress of the unloading soil with true triaxial test method is dramatically larger than that with the latter two tests due to the effect of intermediate principal, which exhibits a nonlinear growth as the coefficient of intermediate principal bd stress jumps. The shear strength indexes of unloading soil with true triaxial test is larger than that with WF stress path test. Compared with the results of routine triaxial test, the internal friction angle of true triaxial test is bigger while the cohesion is smaller.     

大豆堆压缩特性的实验研究

使用TSZ-6A型应变控制式三轴仪对不同围压(8kPa~200kPa)、不同含水率(9.8%、11%、13.5%、14.8%、15.8%w.b.)的黑龙江省大豆堆的体积变化和体变模量进行了测定,分析了围压与含水率对大豆堆体变模量的影响。体变模量随着围压(8kPa~200kPa)的增大而增大,大豆实验结果表明:对含水率为9.8%w.b~15.8%w.b、围压为8kPa~200kPa的大豆堆,其体变模量范围为227.94kPa~610.58kPa。相同含水率的大豆堆的体变模量随着围压(8kPa~200kPa)的增大而增大;同一围压下,大豆堆体变模量随着含水率(9.8%w.b~15.8%w.b)的增大而减小。     

建筑垃圾细料生产流动化回填材料的性能

以灰砂比0.03、0.05和0.08,粉砂比0、0.05、0.1、0.15和0.2为设计参数,对建筑垃圾回填材料进行设计。通过试验对回填材料的流动性(流动度、泌水率)、无侧限抗压强度以及应力应变曲线、本构关系模型和弹性模量等进行研究。研究结果表明:回填材料的流动度受水固比影响较大,两者接近线性关系;流动度在200~250 mm范围,泌水率在4%~8%之间;回填材料抗压强度与灰砂比和水固比之间存在很好的幂指数关系;回填材料应力应变曲线形状与普通混凝土的相似,在此基础上提出回填材料的本构关系模型;回填材料无侧限抗压强度与弹性模量之间存在很好的指数关系。     

Triaxial creep model and its stability analysis of gas containing coal 

Investigation on the creep property of coal containing gas is an effective means for understanding the mechanism of delay outburst of coal and gas in a coal mine. This paper conducts triaxial creep tests on the specimens of gas containing coal using a self made creep experimental apparatus to determine the creep law for coal containing gas. An improved triaxial creep model is developed for containing gas by coupling a Nishihara model with another visco elasto plastic body which can describe the deformation property of non Newtonian fluids. The parameter fittings are conducted based on the experimental dada.The present model is examined in terms to the results of triaxial creep tests in various stress level cases. The result shows that the proposed model for gas containing coal can properly represent the creep deformation at different creep stages, especially at the accelerating stage. The instability condition of the model for coal containing gas is also discussed according to stability theories of differential equation solution.     

Mechanical Properties of Marble at High Temperature

为进一步优化超声波提取胡萝卜中β-胡萝卜紊的工艺条件,在超声功率、超声时间、提取温度、物料粒度、料液比及提取次数6个单因素试验结果的基础上,采用二水平部分因子析因设计（2—level fractional factorial design）法,筛选出了影响β-胡萝卜素提取的主要因素为提取时间（p=0．0145）、温度（p=0．0189）、料液比（p=0．0180）和提取次数（p=0．0114）。     

On the Type of Stress-strain Relation Curves and the Critical State for Soils

In order to discuss the influence of stress history on the constitutive relations for soils,a series of drained conventional triaxial compression tests for normally consolidated and overconsolidated clays have been carried out.It is found through comparing the stress-strain relation curves under the different stress histories that the overconsolidated ratio is the determining factor for volumetric strain.The volumetric strain is less sensitive to consolidation pressure,however.For the shear capacity,the consolidation pressure is the determining factor,but the influence of the overconsolidated ratio can not be neglected since it determines whether there will be strain hardening or strain softening as well as the grade of strain softening.Despite that,the soil specimens will finally reach a unified critical state and approximately the same residual strength.According to the principle of interaction between plastic volumetric and shear strains,the mechanism of generating two types of stress-strain relation curves for clays is explained.It is shown that the critical state is a pure process of shearing deformation in which the interaction between plastic volumetric and shear strains completely disappears.The critical state is independent of the previous stress history.     

The Influence of In-situ Stress Gradient and Geothermal Temperature on The Calculation of Coalbed Gas Pressure

On the basis of coal seam having outcrop of coal seam and outlet on ground,the method for calculating coalbed gas pressure from the one-dimensional stable gas flow equation by considering deeply the influence of in-situ stress gradient and geothermal temperature is presented. In some mine, the theoretically computing and measuring results of coalbed gas pressure show that the in-situ stress gradient and the geothermal temperature have important influence on the calculation of coalbed gas pressure, and if the factors are drew into the calculation of coaled gas pressure,it will make the results much more accurate.     

Clogging mechanical model and its application in gas extraction borehole

A clogging segment mechanical model is established on gas extraction horizontal borehole. Based on the air pressure extremes pmax of the construction site, we solve the corresponding critical clogging length L0 and find clogging will occur when L> L0. With the clogging segment mechanical model, we analyze the calculation method of the retreat drilling rod resistance in borehole. The influence rule of clogging length and air supplying system pressure on retreat drilling rod resistance is analyzed. Analysis results show that the main reason for difficult drilling clogging and retreat drilling rod is the higher pressure in borehole clogging segment. The retreat drilling rod resistance is especially sensitive to the change of air supplying system; therefore, the effective method of reducing the retreat drilling rod resistance is reducing the air supplying system pressure in borehole. The drilling construction status in Jiulishan coal mine is analyzed by using the clogging segment mechanical model, and three technical measures are put forward, including increasing slagging space, reducing slagging resistance and increasing drilling rod strength. When the improving measures are adopted, the pipe-sticking phenomena decreases, the drilling rod broken phenomenon are averted and the drilling efficiency increases by 17%.     

Influences on Engineering Properties of AS Firming Agent Modified Soil by Freeze-thaw Cycles

To study the freeze-thaw durability of Aught-Set(AS) firming agent modified soil, a series of triaxial tests were conducted. The mutual relationships between stress-strain relationship, static strength, dynamic modulus and critical dynamic stress of AS firming agent modified soil and curing time, freeze-thaw cycles, cooling temperature were deeply analyzed. The results show that the unconfined compressive strength of 7 d is 75% than that of 28 d. The stress-strain curves of AS firming-agent modified soil are strain-softening and in brittle failure shape. The static strength, critical dynamic stress and resilient modulus decrease in exponential form with the increase of freeze-thaw cycles, and after 6 cycles of freezing and thawing, the trend is stable. Under the same dynamic stress, the cumulative plastic strain of samples develop from stable state to failure because of freezing and thawing. After many times of freeze-thaw cycles, the lower the negative temperature, the little influence on the mechanic properties.