| 唑虫酰胺15%乳油气相色谱定量分析 |
| |
| 引用本文： | 毕富春,韩冰,王文涛,翟立红,郭奎英,卢亮亮.唑虫酰胺15%乳油气相色谱定量分析[J].农药科学与管理,2012,33(5):41-43. |
| |
| 作者姓名： | 毕富春 韩冰 王文涛 翟立红 郭奎英 卢亮亮 |
| |
| 作者单位： | 1. 南开大学元素有机化学研究所,天津,300071
2. 河北国欣诺农生物技术有限公司,河北河间,062450 |
| |
| 摘 要： | 研究了用大孔径毛细管柱定量分析唑虫酰胺方法。色谱条件如下：DB-115m×0.53×0.5μm。柱温215℃,进样口和检测器温度250℃,载气N2 13mL/min。邻苯二甲酸二癸酯作内标物。本方法在0.625～7.5μg质量的进样范围内和峰面积呈线性。相关系数（R）0.999 8唑虫酰胺分析的回收率为99.95%。
|
| 关 键 词： | 唑虫酰胺 邻苯二甲酸二癸酯 气相色谱法 |
Quantitative Analysis of Tolfenpxrad 15% EC by Gas Chromatography |
| |
| Bi FuchunInstitute of Elemental Organic Chemistry,Nankai University,Tianjin,China Han Bing,Wang Wentao,Zhai Lihong,Guo Kuiying,Lu Liangliang.Quantitative Analysis of Tolfenpxrad 15% EC by Gas Chromatography[J].Pesticide Science and Administration,2012,33(5):41-43. |
| |
| Authors: | Bi FuchunInstitute of Elemental Organic Chemistry Nankai University Tianjin China Han Bing Wang Wentao Zhai Lihong Guo Kuiying Lu Liangliang |
| |
| Institution: | (Hebei guoxinnuonong biotechnology co.,ltd..Hebei Hejian 062450) |
| |
| Abstract: | A method of quantitative analysis for tolfenpxrad by a wide bore capillary column has been studied.Conditions were as follows.Column: 15m×0.53mm×0.5μm DB-1;column temperature: 215℃;temperatures of injector and detector: 250℃,and carried gas: N2 13 mL/min..The 1,2-Benzenedicarboxylicacid,1,2-didecyl ester was used as internal standard.This analytical method is linear and reproducible over the range 0.625 ~7.5μg analyte.A fit these data to a straight line using a least-correlation coefficient yields an R value of 0.9998.The recoveries was 99.95%. |
| |
| Keywords: | tolfenpyrad 1 2-benzenedicarboxylicacid 1 2-didecyl ester gas chroma-tography |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
