| 联苯肼酯43％悬浮剂的高效液相色谱分析 |
| |
| 引用本文： | 肖峥,李海燕,施慧娟,李碧澄.联苯肼酯43％悬浮剂的高效液相色谱分析[J].农药科学与管理,2010,31(8):40-42. |
| |
| 作者姓名： | 肖峥 李海燕 施慧娟 李碧澄 |
| |
| 作者单位： | 1. 上海市质量监督检验技术研究院,上海,200233
2. 上海市农药检定所,上海,201103 |
| |
| 摘 要： | 建立了联苯肼酯悬浮剂的高效液相色谱分析方法。采用Kromasil C18柱．二极管阵列紫外检测器，检测波280nm；以乙腈：0．017mol／L高氯酸水溶液（70：30．v／v）为流动相，流速1．0mL／min。外标法对有效成分进行定量分析，在50—250mg／L范围内线性相关系数为0．99998，平均回收率99．5％，样品测定的标准偏差0．20，变异系数为0．46％。
|
| 关 键 词： | 联苯肼酯 高效液相色谱 分析 |
Analysis of Bifenazate by HPLC |
| |
| Xiao Zheng,Li Haiyan,Shi Huijuan,Li Bicheng.Analysis of Bifenazate by HPLC[J].Pesticide Science and Administration,2010,31(8):40-42. |
| |
| Authors: | Xiao Zheng Li Haiyan Shi Huijuan Li Bicheng |
| |
| Institution: | Xiao Zheng,Li Haiyan,Shi Huijuan(Shanghai Institute of Quality Inspection and TechnicalResearch,Shanghai 200233,China)Li Bicheng(Shanghai Institute for the Control of Agrochemicals,Shanghai 201103,China) |
| |
| Abstract: | An analytical method for the determination of bifenazate established using Kromasil C18 column and DAD detector at 280 nm 43% SC by wavelength. HPLC was The mobile phase was acetonitrile -0.017M perchloric acid solution （70：30, by vol） at a flow rate of 1.0mL/min. The results showed that the linear correlation coefficient was 0.999 9 in the range of 50-250mg/L, the average recovery was 99.5%, the standard deviation was 0.20, the coefficient of variation was 0.46% respectively. |
| |
| Keywords: | bifenazate analysis HPLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
