| 同时分析粮食中敌敌畏等六种有机磷农药气相色谱条件的选择 |
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| 引用本文： | 程兴杰,李万军,李雅莲,陈兆庆. 同时分析粮食中敌敌畏等六种有机磷农药气相色谱条件的选择[J]. 粮食储藏, 2010, 39(1): 49-52 |
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| 作者姓名： | 程兴杰 李万军 李雅莲 陈兆庆 |
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| 作者单位： | 1. 沈阳市粮油检测计量所,110021
2. 大连庄河市粮油检测站,116400 |
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| 摘 要： | 对气相色谱法检测粮食中敌敌畏、敌百虫、马拉硫磷、辛硫磷、杀螟硫磷、甲基嘧啶磷等6种有机磷农药残留量的色谱条件进行优化选择,比较了不同毛细管柱的分离效果,选择了气体的最佳流量和程序升温的最佳起始温度,使保留时间相差很小的组分得到了较好的分离,并提出了解决柱头污染的有效方法。
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| 关 键 词： | 气相色谱 毛细管柱 有机磷农药 |
OPTIMAL SELECTION OF GAS CHROMATOGRAPHY CONDITIONS FOR ANALYZING SIMULTANEOUSLY SIX KINDS OF ORGANOPHOSPHORUS PESTICIDES IN GRAIN |
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| Cheng Xingjie,Li Wanjun,Li Yalian,Chen Zhaoqing. OPTIMAL SELECTION OF GAS CHROMATOGRAPHY CONDITIONS FOR ANALYZING SIMULTANEOUSLY SIX KINDS OF ORGANOPHOSPHORUS PESTICIDES IN GRAIN[J]. www.ysfri.ac.cn, 2010, 39(1): 49-52 |
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| Authors: | Cheng Xingjie Li Wanjun Li Yalian Chen Zhaoqing |
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| Affiliation: | Shenyang Grain&Oils Detection and Measurement Institute 110021;Dalian Zhuanghe Grain&Oils Detection station 116400 |
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| Abstract: | Gas chromatography conditions have been optimally selected for analyzing six kinds of organophosphorus pesticides(including dichlorvos,dipterex,malathion,phoxim,fenitrothion,pirimiphos-methyl) in grain.Separation effects of different capillary columns were compared,the optimal gas flow and original programmed temperature were selected.Compositions with small retention time difference have been separated well,and the effective methods have been put forward to solve the problem of chapiter pollution. |
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| Keywords: | gas chromatography capillary columns organophosphorus pesticide |
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