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长白山特有种单头橐吾的挥发油成分研究
引用本文:董然,南敏伦,刘洪章. 长白山特有种单头橐吾的挥发油成分研究[J]. 安徽农业科学, 2009, 37(36): 17900-17901
作者姓名:董然  南敏伦  刘洪章
作者单位:吉林农业大学园艺学院,吉林长春,130118;吉林省中医药科学院,吉林长春,130118;吉林农业大学生命科学院,吉林长春,130118
基金项目:吉林省科技厅科技支撑项目 
摘    要:[目的]分析长白山特有种单头橐吾叶片挥发油的化学成分。[方法]采用水蒸气蒸馏法提取叶片挥发油,用GC毛细管柱进行分析,用面积归一化法测定其相对含量,并用GC-MS法鉴定化学成分。[结果]检出10个色谱峰,鉴定出9种化合物,占挥发油总量的94.62%。单头橐吾挥发油主要化学成分为石竹烯氧化物(50.00%),其次是植物醇,z-α-反式-香柠檬醇,环戊甲酸-3-异丙叉-龙脑酯,7-亚甲基-2,4,4-三甲基-2-乙烯基-双环[4,3,0]壬烷,3,7-二甲基-6-辛烯-1-醇甲酸酯,而石竹烯和正十六酸的相对含量均在3.00%以下。其中,石竹烯和石竹烯氧化物占总挥发油的52.17%,2种醇类和2种酯类分别占24.00%和10.44%,1种烷类占5.43%。[结论]鉴定出的9种化合物,均首次从该植物中检出,是开发祛痰止咳及强身类药物的重要资源植物。

关 键 词:单头橐吾  挥发油  气相色谱-质谱

Study on the Constituents of Volatile Oils of Changbai Mountain Endemic Species-Ligularia jamesii(Hemsl)Kom.
DONG Ran et al. Study on the Constituents of Volatile Oils of Changbai Mountain Endemic Species-Ligularia jamesii(Hemsl)Kom.[J]. Journal of Anhui Agricultural Sciences, 2009, 37(36): 17900-17901
Authors:DONG Ran et al
Affiliation:DONG Ran et al(College of Horticulture,Jilin Agricultural University,Changchun,Jilin 130118 )
Abstract:[Objective]The chemical constituents of volatile oils of Changbai Mountain endemic species-Ligularia jamesii(Hemsl)Kom.leaves were analyzed.[Method]Steam distillation method was used to extract volatile oils from the leaves,GC capillary column was used to analyze, area normalization method was adopted to determine its relative contents,and GC-MS method was choosed to identify its chemical constituents. [Result]10 chromatographic peaks were detected,and 9 chemical compounds were identified,which accounted fo...
Keywords:Ligularia jamesii (Hemsl)Kom  Volatile oil  Gas chromatography-mass spectrum
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