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毛竹精油和正己烷提取物的GC-MS分析(英文)
引用本文:刘志明,任海青. 毛竹精油和正己烷提取物的GC-MS分析(英文)[J]. 农业科学与技术, 2012, 0(5): 993-996
作者姓名:刘志明  任海青
作者单位:东北林业大学材料科学与工程学院生物质材料科学与技术教育部重点实验室;中国林业科学研究院木材工业研究所
基金项目:Supported by Sub-project of the "Eleventh Five-Year" National Science and Technology Support Program (2006BAD19B04)~~
摘    要:[目的]分析毛竹精油和正己烷提取物的化学组分和得率,寻找潜在价值的活性化合物。[方法]水蒸气蒸馏和正己烷超声波辅助分别提取4个不同竹龄毛竹精油和正己烷提取物,并进行气相色谱/质谱(GC/MS)分析。[结果]结果表明柏木醇(46.39%)是7年毛竹中部精油的第一主要挥发性成分;邻苯二甲酸二丁酯(59.46%)是3年毛竹中部正己烷提取物的第一主要挥发性成分;毛竹正己烷提取物得率高于精油得率。[结论]柏木醇是一种具有潜在价值的活性化合物

关 键 词:毛竹  水蒸气蒸馏  超声波辅助  正己烷  气相色谱/质谱(GC/MS)

GC-MS Analysis of Essential oil and n-Hexane Extract from Moso Bamboo
Zhiming LIU,Haiqing REN. GC-MS Analysis of Essential oil and n-Hexane Extract from Moso Bamboo[J]. Agricultural Science & Technology, 2012, 0(5): 993-996
Authors:Zhiming LIU  Haiqing REN
Affiliation:1.Key Laboratory of Bio-based Material Science and Technology of Ministry of Education,College of Material Science and Engineering,Northeast Forestry University,Harbin 150040,China;2.Research Institute of Wood Industry,Chinese Academy of Forestry,Beijing 100091,China
Abstract:[Objective] This study aimed to analyze the chemical composition and yield of essential oil and n-hexane extract from moso bamboo to find active compounds with potential value.[Method] Essential oil and n-hexane extract were respectively extracted from moso bamboo of four different ages by using hydrodistillation and ultrasonic-assisted extraction with n-hexane,and analyzed with gas chromatography/mass spectrometry(GC/MS).[Result] The results show that cedrol(46.39%) is the first principal volatile component in essential oil of the middle stem of 7-year old moso bamboo;dibutyl phthalate(59.46%) is the first principal volatile component in n-hexane extract of the middle stem of 3-year old moso bamboo;yield of n-hexane extract is higher than that of essential oil from moso bamboo.[Conclusion] Cedrol is an active compound with potential value.
Keywords:Moso bamboo  Hydrodistillation  Ultrasonic assistance  n-hexane extract  Gas chromatography/mass spectrometry(GC/MS)
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