蔬菜中毒死蜱残留量FPD检测的基质效应 |
| |
引用本文: | 黄义彬,郑永林,张建宇.蔬菜中毒死蜱残留量FPD检测的基质效应[J].农技服务,2011,28(3):270-272. |
| |
作者姓名: | 黄义彬 郑永林 张建宇 |
| |
作者单位: | 贵州省贵阳市农产品质量安全监督检验测试中心,贵州贵阳,550008 |
| |
摘 要: | 通过对不同标准溶液配制方式建立校正曲线外标法定量的回收率比较,丙酮基质溶剂配制的毒死蜱标准溶液校正曲线回收率为92%~99%,相对标准偏差(RSD)≤4.18%,毒死蜱在0.035~1.4 mg/L范围内有很好的线性关系,该方法的仪器检出限为0.02 mg/L,方法检出限为0.008 mg/kg.对同一样品采用双火焰光...
|
关 键 词: | 蔬菜 毒死蜱 火焰光度检测器(FPD) 基质效应 |
Chlorpyrifos Residues in Vegetables Detection of Matrix Effects FPD |
| |
Authors: | HUNG Yi-bin |
| |
Institution: | HUNG Yi-bin et al(Guiyang City,Quality and Safety of Agricultural Products Supervision and Testing Center,Guiyang Guizhou 550008) |
| |
Abstract: | The standard solutions prepared by different methods to establish the amount of external standard calibration curve recovery com- pared to the preparation of acetone solvent matrix calibration curve standard solution of chlorpyrifos recovery is 92% to 99% ,relative standard deviation (RSD) ≤4.18% ,chlorpyrifos in the 0. 035 - 1.4 mg/L in the range a good linear relationship between the instrument detection limit of this method is 0.02 mg/L, the detection limit is 0. 008 mg/kg. On the same sample by double flame photometric detector (FPD) detection, DB - 1701 + DG than the DB - 1 column matrix effects a small column. Standard solution prepared by the solvent matrix to establish the amount of external standard calibration curve to eliminate matrix effects. |
| |
Keywords: | Vegetables Chlorpyrifos Flame photometric detector(FPD) Matrix effect |
本文献已被 CNKI 维普 万方数据 等数据库收录! |
|