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等离子发射光谱测定蔬菜矿质元素前处理方法研究
引用本文:刘中笑,徐东辉,张延国,高苹,刘肃. 等离子发射光谱测定蔬菜矿质元素前处理方法研究[J]. 中国蔬菜, 2010, 1(12): 50-54
作者姓名:刘中笑  徐东辉  张延国  高苹  刘肃
作者单位:中国农业科学院蔬菜花卉研究所,北京 100081
摘    要:以黄瓜、大白菜、辣椒、萝卜和菜豆5种蔬菜为试材,对应用等离子发射光谱仪(ICP)测定矿质元素前处理中涉及到的关键因素进行了研究,包括酸介质的选择、标准曲线绘制方法、消化方法、不同样品状态消化等方面。结果表明,由于蔬菜具有新鲜多汁的特性,不同的前处理方法对测定结果有一定的差异。所以要根据样品的不同性状来选择适合的前处理方法,最后获得准确的试验数据。

关 键 词:蔬菜  等离子发射光谱仪法  矿质元素  前处理  
收稿时间:2010-01-20;

Studies on Pre-treatment Method of Determining Mineral Elements in Vegetables by ICP Spectrometer
LIU Zhong-xiao,XU Dong-hui,ZHANG Yan-guo,GAO Ping,LIU Su. Studies on Pre-treatment Method of Determining Mineral Elements in Vegetables by ICP Spectrometer[J]. China Vegetables, 2010, 1(12): 50-54
Authors:LIU Zhong-xiao  XU Dong-hui  ZHANG Yan-guo  GAO Ping  LIU Su
Affiliation:Institute of Vegetables and Flowers, Chinese Academy of Agricultural Sciences, Beijing 100081, China
Abstract:ICP Spectrometric Method is a high-throughput and accuracy optical test for mineral elements determination. Cucumber, Chinese cabbage, pepper, radish and bean were chosen as materials for mineral elements determination by ICP spectrometric method. Some pre-treatment processes including selection of acid media, drawing method of standard curve, digestion method and different sample digesting state were studied. The results showed that appropriate pre-treatment method can cause some differences on the determination results because of the fresh juicy features of the vegetables. Appropriate pre-treatment method was chosen according to different traits of the samples. Thus, accurate experiment data can be acquired.
Keywords:ICP Spectrometric method  Mineral Elements  Pre-treatment
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