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红外光谱法对聚丙烯中抗氧剂168的定量研究
引用本文:陈键,张桂云,梁进杰,林志豪,罗鹏安. 红外光谱法对聚丙烯中抗氧剂168的定量研究[J]. 仲恺农业工程学院学报, 2014, 27(1): 23-26
作者姓名:陈键  张桂云  梁进杰  林志豪  罗鹏安
作者单位:1仲恺农业工程学院化学化工学院
摘    要:利用红外光谱法快速测定了聚丙烯(Polypropylene,PP)中辅助抗氧剂168在加工过程中的消耗量,分别得到了PP/抗氧剂168体系和PP/抗氧剂1010(定量)/抗氧剂168体系中抗氧剂168含量与其特征吸收峰面积的标准曲线,其相关系数均大于0.99.结果表明,样品中抗氧剂168的计算值与测量值相对误差均不超过7%,基本适用于实际检测的需要.

关 键 词:红外光谱  聚丙烯  抗氧剂  定量测定  
收稿时间:2015-10-27

Quantitative determination of antioxidant 168 in polypropylene by infrared spectrometry
CHEN Jian,ZHANG Guiyun,LIANG Jinjie,LIN Zhihao,LUO Pengan. Quantitative determination of antioxidant 168 in polypropylene by infrared spectrometry[J]. Journal of Zhongkai University of Agriculture and Technology, 2014, 27(1): 23-26
Authors:CHEN Jian  ZHANG Guiyun  LIANG Jinjie  LIN Zhihao  LUO Pengan
Affiliation:(College of Chemistry and Chemical Engineering, Zhongkai University of Agricultural and Engineering , Guangzhou 510225, China)
Abstract:For the prediction of polypropylene (PP) in auxiliary antioxidant 168 in the consumption process, characteristic absorption peaks of antioxidant 168 could be fast determined via IR spectrum analysis. The component of one sample was PP with Antioxidants - 168. The following one was PP with antioxidant 1010 and double amount of antioxidant 168. The task was analyzing the content of antioxidant - 168 in this two samples and making the standard curve of antioxidant 168. The standard curve correlation coefficient attained more than 0. 99. The relative error was less than 7% between calculated value as well as measured value and thus demonstrated to satisfy the actual tests.
Keywords:FTIR  Polypropylene  Antioxidants  Quantitative determination
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