荧光光谱滴定法测定痕量的双甲脒 |
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引用本文: | 方晓丽,吴明来,钱一华,张征. 荧光光谱滴定法测定痕量的双甲脒[J]. 安徽农学通报, 2012, 18(15): 158-159 |
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作者姓名: | 方晓丽 吴明来 钱一华 张征 |
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作者单位: | 池州市农产品质量安全监测中心,安徽池州,247000 |
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摘 要: | 通过荧光光谱滴定法研究了脱叔丁基杯[4]芳烃与双甲脒之间的相互作用。实验表明在加入不同量的双甲脒后脱叔丁基[4]芳烃的荧光发生猝灭,由此建立了一种快速简便的测定双甲脒的方法,该方法的线性范围是1.00~60.0μg/mL,添加回收试验表明该方法可行。
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关 键 词: | 双甲脒 脱叔丁基杯[4]芳烃 荧光光谱法 测定 |
The Determination Method of Fluorescence Spectroscopic Titration on Amitraz |
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Affiliation: | Fang Xiaoli et al.(Chizhou Agricultural Products Quality and Safety Monitoring Center,Chizhou 247000,China) |
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Abstract: | The interaction between calix[4]arene and Amitraz was studied by the method of fluorescence spectrometry.It was found that the fluorescence intensity of calix[4]arene regularly decreased upon the addition of amitraz.A novel calix[4]arene-based fluorometic method has been developed for the rapid determination of amitraz with a good linearity in the concentration range between 1.00~60.0μg/mL.The recovery experiment results shows this method is feasible. |
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Keywords: | Amitraz Calix[4]arene Fluorescence spectroscopy Detection |
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