| RP-HPLC测定干姜中6-姜酚的含量 |
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| 引用本文： | 罗少华,邵伟,龚大春.RP-HPLC测定干姜中6-姜酚的含量[J].农产品加工．学刊,2011(12):79-81. |
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| 作者姓名： | 罗少华 邵伟 龚大春 |
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| 作者单位： | 三峡大学化学与生命科学学院,湖北宜昌,443002 |
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| 摘 要： | 采用RP-HPLC法,使用依利特ODS色谱柱(Hypersil,4.6 mm×150 mm,5μm),以乙腈—0.1%醋酸水溶液(55∶45)为流动相,流速1.0 mL/min,检测波长280 nm,柱温35℃,检测干姜中6-姜酚的含量。结果表明,标准曲线线性相关系数R为0.999 8;连续进样5次,测定的峰面积RSD为0.47%;同一样品3次检测结果的最大相对偏差为4.4%;适合于作为干姜中6-姜酚含量的测定方法。
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| 关 键 词： | RP-HPLC 干姜 6-姜酚 |
RP-HPLC Determination of 6-gingerol in Rhizoma Zingiberis |
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| Luo Shaohua,Shao Wei,Gong Dachun.RP-HPLC Determination of 6-gingerol in Rhizoma Zingiberis[J].Nongchanpin Jlagong.Xuekan,2011(12):79-81. |
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| Authors: | Luo Shaohua Shao Wei Gong Dachun |
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| Institution: | (College of Chemistry and Life Science,China Three Gorges University,Yichang,Hubei 443002,China) |
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| Abstract: | Using RP-HPLC method to determine 6-gingerol in Rhizoma Zingiberis,the system consisted of Elite Hypersil ODS column(4.6 mm×150 mm,5 μm),mobile phase of acetonitrile-water with 0.% acetic acid(55∶45) mixture,with a flow rate of 1.0 mL/min,detection at 280 nm,column temperature of 35 ℃.The results show that the correlation coefficient of the determination is 0.999 8,the method has high precision with RSD as 0.47% for the continuous feeding 5 times.This method is suitable for the determination of 6-gingerol. |
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| Keywords: | HPLC Rhizoma Zingiberis 6-gingerol |
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