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1%噻虫啉粉剂液相色谱分析方法研究
引用本文:王英爽,葛迎春,韩冰,卢洪斌.1%噻虫啉粉剂液相色谱分析方法研究[J].防护林科技,2014(3):32-33.
作者姓名:王英爽  葛迎春  韩冰  卢洪斌
作者单位:黑龙江省平山林业制药厂,黑龙江哈尔滨150324
摘    要:采用液相色谱法,用可变波长紫外检测器和C18反相色谱柱,以甲醇、乙腈和水为流动相,对粉剂中的噻虫啉进行检测。结果表明:分析方法的线性相关系数为0.999 5,标准偏差为0.013,变异系数为1.29%,1%噻虫啉的平均回收率达99.88%。

关 键 词:噻虫啉  液相色谱法  检测

Determination of 1% Thiacloprid Powder By HPLC
Wang Yingshuang,Ge Yingchun,Han Bing,Lu Hongbin.Determination of 1% Thiacloprid Powder By HPLC[J].Protection Forest Science and Technology,2014(3):32-33.
Authors:Wang Yingshuang  Ge Yingchun  Han Bing  Lu Hongbin
Institution:(Heilongjiang Pingshan Forestry Pharmaceutical Factory, Harbin 150324,China)
Abstract:Taking liquid chromatography ,using a variable wavelength UV detector and a C18 reverse phase column , taking methanol ,acetonitrile & water as the mobile phase ,thiacloprid of powders were determined .Result shows that :the linear correlation coefficient is 0 .999 5 ,standard deviation being 0 .013 ,the coefficient of variation being 1 . 29% ,the mean recovery rate of 1% thiacloprid being 99 .88% .
Keywords:thiacloprid  liquid chromatography  determination
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