| 马拉硫磷对照品的制备 |
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| 引用本文： | 温芳,张秀英,郭桂芳,陆连寿,郝利华. 马拉硫磷对照品的制备[J]. 中国兽药杂志, 2021, 55(1): 20-24 |
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| 作者姓名： | 温芳 张秀英 郭桂芳 陆连寿 郝利华 |
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| 作者单位： | 中国兽医药品监察所,,,, |
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| 摘 要： | 通过对马拉硫磷对照品候选物进行全面质量控制,以美国药典委员会提供的马拉硫磷对照品作为溯源对照品,用高效液相方法通过协作标定对制备的马拉硫磷对照品进行定值,确定制备马拉硫磷对照品含量为99.0%,相对标准偏差为0.3%。通过对马拉硫磷对照品的研制,期望能对兽用化学药品对照品的研制提供一些参考意见和建议。
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| 关 键 词： | 马拉硫磷 对照品 定值 |
| 收稿时间： | 2020-09-18 |
| 修稿时间： | 2020-10-15 |
Preparation of malathion reference substance |
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| WEN Fang,ZHANG Xiu-ying,LU Lian-shou,GUO Gui-fang,WAN Ren-ling,HAO Li-hua,GONG Zhong-fu. Preparation of malathion reference substance[J]. Chinese Journal of Veterinary Drug, 2021, 55(1): 20-24 |
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| Authors: | WEN Fang ZHANG Xiu-ying LU Lian-shou GUO Gui-fang WAN Ren-ling HAO Li-hua GONG Zhong-fu |
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| Affiliation: | Chinese Institute of Veterinary Drug Control,,,, |
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| Abstract: | We subject the malathion candidate materials to comprehensive quality control checks.Testing USP malathion reference substance as a traceable reference,and determine the content of malathion candidate materials using HPLC method by collaborative testing.the average content of malathion candidate materials was 99.0%with RSD of 0.3%.it would help for the research and preparation reference substance of veterinary chemical drug. |
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| Keywords: | malathion reference substance determination content |
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