| 超临界CO_2流体萃取分离高纯栀子甙的工艺研究 |
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| 引用本文： | 余顺火,李先祥,马道荣,章建国. 超临界CO_2流体萃取分离高纯栀子甙的工艺研究[J]. 农产品加工．学刊, 2008, 0(12) |
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| 作者姓名： | 余顺火 李先祥 马道荣 章建国 |
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| 作者单位： | 1. 合肥工业大学生物与食品工程学院,安徽合肥,230009
2. 安徽省毫州市亚强天然产物制品厂,安徽毫州,236800 |
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| 摘 要： | 采用超临界CO2流体萃取分离技术,对栀子黄提取废液中的栀子甙进行分离精制。分别考察了分离温度和分离压力对栀子甙和栀子黄分离效果的影响,在此基础上对超临界CO2流体萃取的分离工艺进行了改进。实验结果表明,降低分离压力有利于对栀子甙和栀子黄的分离,分离温度低于40℃时,升高温度有利于栀子甙分离而不利于栀子黄分离;分离温度在高于40℃时,对二者分离均不利。改进后的"一萃两分"工艺最佳分离工艺参数为:分离压力均为8MPa,第1次分离温度为40℃,第2次分离温度为25℃。
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| 关 键 词： | 超临界CO2流体 栀子甙 分离 |
Study on the Extraction Technology of High-quality Gardenoside by Supercritical CO_2 Fluid |
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| Yu Shunhuo,Li Xianxiang,Ma Daorong,Zhang Jianguo. Study on the Extraction Technology of High-quality Gardenoside by Supercritical CO_2 Fluid[J]. Nongchanpin Jlagong.Xuekan, 2008, 0(12) |
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| Authors: | Yu Shunhuo Li Xianxiang Ma Daorong Zhang Jianguo |
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| Affiliation: | Yu Shunhuo1,Li Xianxiang2,Ma Daorong1,Zhang Jianguo1 (1. The School of Biotechnology , Food Engineering,Hefei University of Technology,Hefei,Anhui 230009,China,2. Yaqiang Natural Product Factory,Bozhou,Anhui 236800,China) |
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| Abstract: | Gardenoside was extracted and refined from exhausted solution of gardenia yellow with supercritical CO2 fluid (SCF) technique. Firstly, it had been detected respectively that the influence of temperature and pressure on the gardenoside purification during the process that gardenoside was separated from the exhausted solution. Then,the extract technology of SCF was improved based on the above test and induced the follow conclusions: Low pressure can benefit the separate of gardenoside and gardenia yellow;whe... |
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| Keywords: | supercritical CO2 fluid gardenoside separation |
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