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有机肥料中钠含量检测技术研究
引用本文:杜颖,马良,白杨,刘善江.有机肥料中钠含量检测技术研究[J].湖北农业科学,2017,56(6).
作者姓名:杜颖  马良  白杨  刘善江
作者单位:1. 北京市农林科学院植物营养与资源研究所,北京,100097;2. 北京市农林科学院植物营养与资源研究所,北京 100097;农产品产地环境监测北京市重点实验室,北京 100097
基金项目:北京市农林科学院科技创新能力建设专项,农产品质量与农田环境基础数据平台建设项目
摘    要:有机肥料试样经硫酸和过氧化氢消煮后过滤,过滤液分别用火焰光度法和ICP-OES法测定。结果表明,火焰光度法与ICP-OES法均能得到较好的试验结果,火焰光度法的测定值高于ICP-OES法,二者相对相差小于30%,火焰光度法和ICP-OES法的回收率分别为101.0%和99.0%,RSD分别为1.0%和0.3%,说明两种方法测定全钠具有较好的准确度和精密度,而ICP-OES法对批量样品的检测更具优势。

关 键 词:有机肥料  全钠  火焰光度法  ICP-OES法

Study on Detection of Sodium in Organic Fertilizers
DU Ying,MA Liang,BAI Yang,LIU Shan-jiang.Study on Detection of Sodium in Organic Fertilizers[J].Hubei Agricultural Sciences,2017,56(6).
Authors:DU Ying  MA Liang  BAI Yang  LIU Shan-jiang
Abstract:Organic fertilizer samples were digested by sulfuric acid and hydrogen peroxide. Then filtrate were determinate by flame photometer and ICP-OES respectively. The results showed that flame photometer and ICP-OES could can get a better test results, Flame photometer measurement value is higher than ICP-OES method, the results of the relative difference be-tween the two methods was not more than 30%. The recovery rate of the two methods which was flame photometer and ICP-OES were 101.0% and 99.0%, RSD values were 1.0% and 0.3% respectively. Comparing the measured results showed that both methods had good accuracy and precision. The ICP-OES method had more advantages for the detection of bulk samples.
Keywords:organic fertilizer  sodium  flame photometer method  ICP-OES method
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