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气相色谱法检测茶叶中噻嗪酮(优乐得)和菊酯类农药的残留量
引用本文:于萍萍,谢涛,唐文,张进忠.气相色谱法检测茶叶中噻嗪酮(优乐得)和菊酯类农药的残留量[J].山东农业科学,2007(3):99-101.
作者姓名:于萍萍  谢涛  唐文  张进忠
作者单位:1. 西南大学资源环境学院,重庆,400716;重庆市农业资源与环境重点实验室,重庆,400716
2. 西南大学资源环境学院,重庆,400716
3. 四川省南充炼油化工总厂,四川南充,637000
4. 重庆市农业资源与环境重点实验室,重庆,400716
摘    要:利用配有电子捕获检测器(ECD)的气相色谱仪测定了茶叶中噻嗪酮(优乐得)、甲氰菊酯、氰戊菊酯、联苯菊酯的残留,结果4种农药的检出限量分别为0.01、0.01、0.05、0.01 mg/kg,加标回收率分别为86.0%~100.5%、84.7%~99.3%、83.3%~100.2%、87.3%~100.5%,且变异系数均在2.1%~4.6%范围内,表明该方法的准确度、灵敏度、精密度均较高。

关 键 词:气相色谱  茶叶  残留  菊酯类农药  噻嗪酮(优乐得)
文章编号:1001-4942(2007)03-0099-03
修稿时间:2007-01-092007-04-04

Residual Determination of Buprofezin and Chrysanthemum Ester Pesticides in Tea by GC
YU Ping-ping,XIE Tao,TANG Wen,ZHANG Jin-zhong.Residual Determination of Buprofezin and Chrysanthemum Ester Pesticides in Tea by GC[J].Shandong Agricultural Sciences,2007(3):99-101.
Authors:YU Ping-ping  XIE Tao  TANG Wen  ZHANG Jin-zhong
Institution:1. College of Resources and Enviroment , Southwest University, Chongqing 400716 ,China ; 2. Chongqing Key Laboratory of Agricultural Resources and Environment, Chongqing 400716, China ; 3. Sichuan Industrial Complex of the Oil Refining Chemical Engineering in Nanchong City,Nanchong 637000, China
Abstract:The residual contents of Buprofezin, Fenpropathrin, Fenvalerate and Bifenthrin in tea were determined by GC with ECD. The results showed that their detection limits were 0.01 mg/kg, 0.01 mg/kg,0. 05 mg/kg and 0.01 mg/kg,respectively. Their recovery rates were 86.0-100. 5%, 84. 7-99.3% ,83. 3%-100. 2% and 87. 3%-100. 5% ,respectively,and their variation coefficients were in 2. 1-4.6%. So the accuracy,sensibility and precision of this method was higher.
Keywords:GC  Tea  Residue  Chrysanthemum ester pesticides Buprofezin
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