| 液相色谱法测定食品中抗氧化剂特丁基对苯二酚 |
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| 引用本文： | 桂学琴. 液相色谱法测定食品中抗氧化剂特丁基对苯二酚[J]. 安徽农业科学, 2007, 35(6): 1577-1577,1584. DOI: 10.3969/j.issn.0517-6611.2007.06.003 |
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| 作者姓名： | 桂学琴 |
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| 作者单位： | 安徽大学现代实验技术中心,安徽合肥,230039 |
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| 摘 要： | 采用高效液相色谱法测定食品中的抗氧化剂特丁基对苯二酚(TBHQ).样品经甲醇提取过滤后测定,检测波长为280 nm,流动相为乙腈-水(含1%的乙酸,体积比为 45∶55),结果表明,TBHQ回收率大于85%,测定结果的相对标准偏差小于2%.该方法简单、快捷、准确,可广泛应用于油脂及多种食品中TBHQ的检测.
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| 关 键 词： | 食品 特丁基对苯二酚 抗氧化剂 高效液相色谱 |
| 文章编号： | 0517-6611（2007）06-01577-01 |
| 修稿时间： | 2006-12-06 |
Determination of Antioxidant TBHQ in Food by HPLC |
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| GUI Xue-qin. Determination of Antioxidant TBHQ in Food by HPLC[J]. Journal of Anhui Agricultural Sciences, 2007, 35(6): 1577-1577,1584. DOI: 10.3969/j.issn.0517-6611.2007.06.003 |
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| Authors: | GUI Xue-qin |
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| Affiliation: | Center of Modem Experiment and Technology, Anhui University, Hefei, Anhui 230039 |
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| Abstract: | A HPLC procedure was developed for the determination of tertiary butylhydroquinone(TBHQ) in food.After the sample was extracted with methanol and filtered it can be determined with HPLC.The detect wavelength was 280 nm,and the mobile phase was acetonitrile and H2O(the ratio of volume was 45∶55).The recovery of the TBHQ was upwards 85% and the relative standard deviation was less than 2%.The facile method was efficient,accurate and suitable for routine analysis of TBHQ in oil and foods. |
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| Keywords: | Foods Butylhydroquinone(TBHQ) Antioxidant HPLC |
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