| 超高效液相色谱—串联质谱法快速检测水中氟蚁腙的残留 |
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| 引用本文： | 朴秀英,郭子靖,周艳明,王晓军,姜辉.超高效液相色谱—串联质谱法快速检测水中氟蚁腙的残留[J].农药科学与管理,2012,33(10):27-29. |
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| 作者姓名： | 朴秀英 郭子靖 周艳明 王晓军 姜辉 |
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| 作者单位： | 农业部农药检定所,北京,100125 |
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| 摘 要： | 建立了水样品中氟蚁腙残留的超高效液相色谱-串联质谱检测方法。水样品用正己烷和丙酮的混合溶液提取,用UPLC-MS/MS测定。氟蚁腙在水中的平均回收率和RSD分别为91.8～93.2%和2.78～6.02%。该检测方法具有灵敏度高、快速、操作简单等特点,并可用于水样品中氟蚁腙的检测。
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| 关 键 词： | 氟蚁腙 超高效液相色谱-串联质谱 水 |
Simplified Method for Determination of Hydramethylnon Residues in Water using UPLC-MS/MS |
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| Piao Xiuying,Guo Zijing,Zhou Yanming,Wang Xiaojun,Jiang Hui.Simplified Method for Determination of Hydramethylnon Residues in Water using UPLC-MS/MS[J].Pesticide Science and Administration,2012,33(10):27-29. |
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| Authors: | Piao Xiuying Guo Zijing Zhou Yanming Wang Xiaojun Jiang Hui |
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| Institution: | (Institute for the Control of Agrochemicals,Ministry of Agriculture,Beijing 100125,China) |
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| Abstract: | The analysis method of hydramethylnon in water was established using UPLC-MS/MS.The water sample were extracted by the mixture of hexane and acetone then determined by UPLC-MS/MS.The average recoveries rate and RSD of hydramethylnon in water were 91.8～93.2% and 2.78～6.02% respectively.The method was sensitive,rapid and simple so that reliable to determine the hydramethylnon residues in water. |
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| Keywords: | hydramethylnon UPLC-MS/M S water |
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