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Isolation, identification and dyeing studies of betanin on modified acrylic fabrics
Authors:A Guesmi  N LadhariN Ben Hamadi  F Sakli
Institution:a Textile Research Unit, Higher Institute of Technological Studies of Ksar Hellal, Tunisia
b Laboratory of Synthesis Heterocyclic and Natural Substances, Monastir, Tunisia
Abstract:Mature red fruits of Opuntia ficus-indica contain two soluble pigment, betanin and indicaxanthin. The optimal conditions for dye extraction were to mix 50 g of juice from cactus pears with 100 mL of acidified water as solvent for dye extraction. Two main dyes were purified from the pigment extract by chromatography and identified by UV-vis, HPLC and LC-MS techniques as indicaxanthin (15 mg per 100 g) and betanin (280 mg per 100 g). The effect of dye bath pH, salt concentration, dyeing time and temperature was studied. The optimal conditions for dyeing modified acrylic fabrics with betanin dye were carried out at 50 °C for 45 min at pH 5. Un-mordanted samples have good properties of water and washing fastness. Mordant CoSO4 was found to give good light fastness (rating 5).
Keywords:Opuntia ficus-indica  Betanin  Natural dye  Modified acrylic  Mordant  Fastness
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