| 青饲料中氨基甲酸酯类农药残留的高效液相色谱法测定 |
| |
| 引用本文： | 张蓉琴,方晓燕,叶一,王丽敏,张静恒.青饲料中氨基甲酸酯类农药残留的高效液相色谱法测定[J].四川畜牧兽医,2013(12):26-28. |
| |
| 作者姓名： | 张蓉琴 方晓燕 叶一 王丽敏 张静恒 |
| |
| 作者单位： | 四川省成都市食品药品检测中心,四川成都610041 |
| |
| 摘 要： | 本试验建立了一种简便而准确的前处理方法——高效液相色谱法,用于检测青饲料中7种氨基甲酸酯类农药的残留.用高效液相色谱法紫外检测器测定多菌灵,用高效液相色谱柱后衍生系统荧光检测器测定克百威或3-羟基克百威、涕灭威或涕灭威砜、涕灭威亚砜及甲萘威.结果显示：青饲料中7种农药的加标回收率（n=6）在73.2％～98.3％,RSD在2.1％～6.9％,方法的检出限（以3倍信噪比计）为0.19～0.90 μg/kg.
|
| 关 键 词： | 氨基甲酸酯 高效液相色谱 柱后衍生 青饲料 |
Study on the Detection of Carbamates Pesticides in Green Fodder by HPLC |
| |
| Institution: | ZHANG Rong-qin FANG Xiao-yan YE Yi(Chengdu Food and Drug Testing Center in Sichuan Province,Sichuan Chengdu 610041, China) |
| |
| Abstract: | A simple and repeatable pretreatment method was set up by HPLC using uv detector to detect carbendazim, using post-column derivatization system and fluorescence detector to detect other six carbamates pesticides in green fodder. The spiked recoveries varied from 73.2% to 98.3% with relative standard deviations of 2.1%-6.9%, the limits of detection （S/N=3） varied from 0.19μg/kg to 0.90μg/kg. The proposed method was sensitive and highly efficient. |
| |
| Keywords: | Carbamates pesticides HPLC Post-column derivatization Green fodder |
| 本文献已被 维普 等数据库收录！ |
|
