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超声波辅助提取胡椒中胡椒碱
引用本文:陈盛余,赵丹丹,曾小月,史兵方,凌绍明,谢瑜.超声波辅助提取胡椒中胡椒碱[J].湖北农业科学,2017,56(5).
作者姓名:陈盛余  赵丹丹  曾小月  史兵方  凌绍明  谢瑜
作者单位:广西高校桂西生态环境分析和污染控制重点实验室/百色学院,广西 百色,533000
基金项目:广西高等学校优势特色专业建设项目,百色学院校级科学研究项目,广西大学生创新训练项目
摘    要:采用单因素和正交试验优化从胡椒(Piper nigrum L.)中提取胡椒碱的工艺条件,分别考察了料液比、乙醇体积分数、提取时间和提取温度对胡椒碱提取率的影响。结果表明,胡椒碱的最佳提取工艺为料液比1∶30(g∶m L),乙醇体积分数95%,提取时间45 min,提取温度70℃。在最佳条件下,胡椒碱提取率达到6.12%。该提取工艺简单、高效,可以应用于从胡椒中提取胡椒碱。

关 键 词:胡椒(Pipernigrum  L.)  胡椒碱  超声波提取  正交试验

Ultrasonic Extraction Piperine from Piper nigrum L.
CHEN Sheng-yu,ZHAO Dan-dan,ZENG Xiao-yue,SHI Bing-fang,LING Shao-ming,XIE Yu.Ultrasonic Extraction Piperine from Piper nigrum L.[J].Hubei Agricultural Sciences,2017,56(5).
Authors:CHEN Sheng-yu  ZHAO Dan-dan  ZENG Xiao-yue  SHI Bing-fang  LING Shao-ming  XIE Yu
Abstract:The extracting piperine of Piper nigrum L. was optimized by single-factor experiments. The effects of solid-to-liq-uid ratio,ethanol concentration, extraction time and extraction temperature were investigated respectively. The results showed that optimum extraction process were solid-to-liquid ratio of 1:30 (g:mL),95% ethanol,extraction time of 45 minutes and ex-traction temperature of 70℃. The extraction rate of piperine could reach 6.12% under the optimum conditions. The extraction process was simple,efficient and suitable for extracting piperine of Piper nigrum L.
Keywords:Piper nigrum L    piperine  ultrasonic extraction  orthogonal test
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