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异噁唑草酮原药分析方法
引用本文:迟志娟,邢诗唅,王蓓,王姣,王淳纯,母昌立. 异噁唑草酮原药分析方法[J]. 安徽农业科学, 2016, 44(20): 143-144. DOI: 10.3969/j.issn.0517-6611.2016.20.046
作者姓名:迟志娟  邢诗唅  王蓓  王姣  王淳纯  母昌立
作者单位:江苏省太仓市农产品质量监督检验测试中心,江苏太仓,215412;中国农业大学烟台研究院,山东烟台,264000
摘    要:[目的]建立异噁唑草酮原药的高效液相色谱分析方法。[方法]采用高效液相色谱法,以乙腈-乙酸(55∶45,V/V)为流动相,应用C18色谱柱和SPD-M20A PDA检测器分析异噁唑草酮的含量。[结果]该色谱分析条件下异噁唑草酮的标准偏差为0.008,变异系数为0.09%,回收率为104%。[结论]该方法适用于定性、定量分析异噁唑草酮原药。

关 键 词:异噁唑草酮  高效液相色谱  分析方法

Analysis Method of Isoxaflutole TC
Abstract:Objective] To establish an analysis method for the high performance liquid chromatography (HPLC) of isoxaflutole TC.[Method] High performance liquid chromatography was adopted.With acetonitrile : acetic acid (55∶45, V/V) as the mobile phase, C18 chromatographic column and SPD-M20A PDA detector were used to analyze the content of isoxaflutole.[ Result] Under the chromatographic analysis conditions, the standard deviation of isoxaflutole was 0.008, the variation coefficient was 0.09%, and the recovery rate was 104%.[Conclusion] This meth-od is suitable for the qualitative and quantitative analysis of isoxaflutole TC.
Keywords:Isoxaflutole  High performance liquid chromatography  Analysis method
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