异噁唑草酮原药分析方法 |
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引用本文: | 迟志娟,邢诗唅,王蓓,王姣,王淳纯,母昌立. 异噁唑草酮原药分析方法[J]. 安徽农业科学, 2016, 44(20): 143-144. DOI: 10.3969/j.issn.0517-6611.2016.20.046 |
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作者姓名: | 迟志娟 邢诗唅 王蓓 王姣 王淳纯 母昌立 |
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作者单位: | 江苏省太仓市农产品质量监督检验测试中心,江苏太仓,215412;中国农业大学烟台研究院,山东烟台,264000 |
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摘 要: | [目的]建立异噁唑草酮原药的高效液相色谱分析方法。[方法]采用高效液相色谱法,以乙腈-乙酸(55∶45,V/V)为流动相,应用C18色谱柱和SPD-M20A PDA检测器分析异噁唑草酮的含量。[结果]该色谱分析条件下异噁唑草酮的标准偏差为0.008,变异系数为0.09%,回收率为104%。[结论]该方法适用于定性、定量分析异噁唑草酮原药。
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关 键 词: | 异噁唑草酮 高效液相色谱 分析方法 |
Analysis Method of Isoxaflutole TC |
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Abstract: | Objective] To establish an analysis method for the high performance liquid chromatography (HPLC) of isoxaflutole TC.[Method] High performance liquid chromatography was adopted.With acetonitrile : acetic acid (55∶45, V/V) as the mobile phase, C18 chromatographic column and SPD-M20A PDA detector were used to analyze the content of isoxaflutole.[ Result] Under the chromatographic analysis conditions, the standard deviation of isoxaflutole was 0.008, the variation coefficient was 0.09%, and the recovery rate was 104%.[Conclusion] This meth-od is suitable for the qualitative and quantitative analysis of isoxaflutole TC. |
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Keywords: | Isoxaflutole High performance liquid chromatography Analysis method |
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