泰乐菌素药渣残留量的测定 |
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引用本文: | 王玲,马吉锋,张霞,马玉龙.泰乐菌素药渣残留量的测定[J].现代农业科技,2009(23):337-338. |
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作者姓名: | 王玲 马吉锋 张霞 马玉龙 |
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作者单位: | 1. 宁夏大学化学化工学院,宁夏银川,750021 2. 宁夏农林科学院草畜工程技术研究中心 |
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摘 要: | 采用高效液相色谱-紫外检测方法,建立了泰乐菌素药渣残留量测定的分析方法。泰乐菌素在6min内完全检出。线性范围为0.5~20.0mg/L,相关系数为0.999 8,最小检出浓度为0.1mg/L。将该方法应用于泰乐菌素测定上,回收率介于98.3%~100.3%,效果较好。
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关 键 词: | 泰乐菌素 药渣 残留量 高效液相色谱 紫外检测 |
Determination of residues of Tylosin Dregs |
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Authors: | WANG Ling MA Ji-feng ZHANG Xia MA Yu-long |
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Institution: | WANG Ling , MA Ji-feng , ZHANG Xia , MA Yu-long (1 College of Chemistry and Chemical Engineafing, Ningxia umversity,Yinchuan Ningxia 750021 ; 2 Grass and Live stock Engineering Technology Research Centre, Ningxia Academy of Agriculture and Forestry Sciences) |
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Abstract: | Using the high-performance liquid chromatography(HPLC) with UV detection,a method to detect the residues of tylosin dregs was established.The tylosin was detected comptetely within 6 minutes.The liner ranges were from 0.5mg/L to 20.0mg/L,the correlation coefficient was 0.999 8,and the detection lower limit was 0.1mg/L.The method was exploited to determinate the tylosin dregs samples,and the average spiked recoveries ranged from 98.3% to 100.3% with a good result obtained. |
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Keywords: | tylosin dregs residues high-performance liquid chromatography ultraviolet examination |
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