| HPLC法测定气血康口服液中黄芪甲苷的含量 |
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| 引用本文： | 陶尚贵,张文斌,周家明,曾鸿超. HPLC法测定气血康口服液中黄芪甲苷的含量[J]. 特产研究, 2010, 32(2): 64-65,73 |
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| 作者姓名： | 陶尚贵 张文斌 周家明 曾鸿超 |
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| 作者单位： | 1. 白药集团文山七花有限责任公司质量部,云南文山,663000
2. 文山三七研究院,云南文山,663000 |
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| 摘 要： | 建立气血康口服液中黄芪甲苷含量测定的方法。采用ZORBAXEclipse XDB-C18(4.6×150mm,5μm)色谱柱;流动相为:乙腈∶水(30∶70);流速:1.0mL/min;检测器波长:203nm。结果表明,黄芪甲苷在2~10μg范围内呈良好的线性关系(r=0.999 8,n=5),平均回收率:97.25%,RSD0:.41%。该方法简单、快速、准确,可作为产品的质量控制方法。
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| 关 键 词： | HPLC 气血康口服液 黄芪甲苷 含量测定 |
Determination of Astragaloside IV Content in the Qi and Blood Oral Solution by Using HPLC |
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| TAO Shang-gui,ZHANG Wen-bin,ZHOU Jia-ming,ZENG Hong-chao. Determination of Astragaloside IV Content in the Qi and Blood Oral Solution by Using HPLC[J]. Special Wild Economic Animal and Plant Research, 2010, 32(2): 64-65,73 |
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| Authors: | TAO Shang-gui ZHANG Wen-bin ZHOU Jia-ming ZENG Hong-chao |
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| Affiliation: | 1.Wenshan Yunnan Baiyao Group of Seven Limited Liability Companies Spend Quality Assurance of the Wenshan 663000,China;2.Wenshan Research Institute of Sanqi,Wenshan 663000,China) |
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| Abstract: | To establish measurement method for astragaloside contents in Oral Liquid qi and blood.ZORBAX Eclipse XDB-C18（4.6 ×150mm,5μm） column;mobile phase：acetonitrile：wate（r30∶70）,flow rate： 1.0 ml/min;detector wavelengths：203nm.The AstragalosideIV of 2~10μg within the framework showed a good linear relationship（r = 0.999 8,n = 5）,the average recovery rate： 97.25%,RSD：0.41%,The method is simple,fast and accurate,which can be used as a quality control method for the product. |
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| Keywords: | HPLC |
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