光声光谱法检测生菜中的敌敌畏残留 |
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引用本文: | 龚瑞昆,郑学丽. 光声光谱法检测生菜中的敌敌畏残留[J]. 湖北农业科学, 2016, 0(7): 1812-1814. DOI: 10.14088/j.cnki.issn0439-8114.2016.07.048 |
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作者姓名: | 龚瑞昆 郑学丽 |
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作者单位: | 河北联合大学电气工程学院,河北 唐山,063009 |
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基金项目: | 国家自然科学基金项目(61171058) |
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摘 要: | 为给蔬菜的农药残留检测提供一种快速有效的方法,配置不同浓度的敌敌畏样本,用光声光谱法测定,光谱扫描范围为300~800 nm,调制频率为8~200 Hz。结果表明,利用光声光谱法对生菜中的敌敌畏残留进行检测,线性范围在0.014~0.885μg/m L之间,相关系数r=0.998 5,检出限为0.012μg/m L,与气相色谱法相比无明显差异且测量结果较精确。
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关 键 词: | 光声光谱 敌敌畏 农药残留 生菜 |
Determination for Dichlorvos Pesticide Residual in Lettuce Based on Photoacoustic Spectroscopy Method |
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Abstract: | In order to provide an rapid and effective determination method for pesticide residues in vegetables, pesticide sam-ples with different concentrations of dichlorvos configuration were collected and measured by using the photoacoustic spec-troscopy with spectral scanning range of 300~800 nm and modulation frequency of 8~200 Hz. The results showed that the cor-relation coefficient r=0.9985,the linear range was in 0.014~0.885μg/ml and the detection limit was 0.012μg/ml. There was no obvious difference compared with gas chromatography, and the measurement result was more accurate. |
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Keywords: | photoacoustic spectroscopy dichlorvos pesticide residues Lettuce |
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