| 新型主链杯[4]聚硅氧烷毛细管气相色谱固定相的研究 |
| |
| 引用本文： | 吕全建,刘淑娜,童岩. 新型主链杯[4]聚硅氧烷毛细管气相色谱固定相的研究[J]. 郑州牧业工程高等专科学校学报, 1999, 0(4) |
| |
| 作者姓名： | 吕全建 刘淑娜 童岩 |
| |
| 作者单位： | 郑州牧专基础部，郑州牧专基础部，郑州牧专基础部 郑州 450008，郑州 450008，郑州 450008 |
| |
| 摘 要： | 选用硅氢加成试剂(CH3)2SiHCl,合成了一种主链杯[4]芳烃二丁醚聚硅氧烷毛细管气相色谱固定相,考察了该固定相的色谱特性:柱效、极性、选择性和热稳定性,结果表明该杯[4]芳烃固定相具有良好的色谱性能。异物醇及十种芳香族位置异构体均得到良好分离。
|
| 关 键 词： | 毛细管气相色谱 杯[4]芳烃 固定相 |
A Kind of main chain calix[4]arene polylloxane as capillary gas chromatography stationary phases |
| |
| Abstract: | A kind of main chain calix[4] polylloxane gas stationary phase wes synthesized. The chromatographic characteristics, including column efficiency, polarity, selectivity and thermal stability were studied. The calix[4] ploylloxane stationary phases was found to have unique selectivity for alcohol isomers and positional isomer of derivative compounds. |
| |
| Keywords: | capillary gas chromatography calix[4]arene stationary phase |
| 本文献已被 CNKI 等数据库收录！ |
