| 蔬菜中氟铃脲·氟苯脲·氟虫脲和氟啶脲的高效液相色谱分析 |
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| 引用本文： | 李敏,秦金平,徐春祥. 蔬菜中氟铃脲·氟苯脲·氟虫脲和氟啶脲的高效液相色谱分析[J]. 安徽农业科学, 2011, 39(1): 204-205 |
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| 作者姓名： | 李敏 秦金平 徐春祥 |
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| 作者单位： | 南京工业大学化学化工学院;江苏省产品质量监督检验中心所; |
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| 基金项目： | 江苏省产品质量监督检验中心所2008年度江苏省农业地方标准申报项目 |
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| 摘 要： | [目的]建立蔬菜中氟铃脲、氟苯脲、氟虫脲和氟啶脲4种苯甲酰脲类农药残留的高效液相色谱（HPLC）分析方法。[方法]芹菜、芜菁、萝卜和卷心菜试样经乙腈提取、石油醚和丙酮萃取、弗罗里硅土柱吸附净化后,进行高效液相色谱测定。[结果]该方法的回收率均大于80%,氟铃脲、氟苯脲、氟虫脲和氟啶脲的最低检出限分别为0.04、0.05、0.04和0.03mg/L。[结论]该方法分离效果好,价格低廉,操作简便。
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| 关 键 词： | 苯甲酰脲类农药残留 高效液相色谱法 蔬菜 |
Determination of Hexaflumuron, Teflubenzuron, Flufenoxuron and Chlorfluazuron in Vegetable by HPLC |
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| LI Min et al. Determination of Hexaflumuron, Teflubenzuron, Flufenoxuron and Chlorfluazuron in Vegetable by HPLC[J]. Journal of Anhui Agricultural Sciences, 2011, 39(1): 204-205 |
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| Authors: | LI Min et al |
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| Affiliation: | LI Min et al (College of Chemistry and Chemical Engineering,Nanjing University of Technology,Nanjing,Jiangsu 210009) |
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| Abstract: | [Objective] The aim was to develop a high performance liquid chromatography(HPLC) method for the simultaneously determination of 4 benzoylirea insecticides residues including hexaflumuron,teflubenzuron,flufenoxuron and chlorfluazuron in vegetables.[Method] The vegetable samples including celery,turnip,radish and cabbage were extracted with acetonitrile,further cleaned-up by petroleum ether and acetone,cleaned-up by florisil column,and then determined by HPLC.[Result] Recovery rate of the method was over 80%... |
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| Keywords: | Benzoylirea insecticides residues HPLC Vegetable |
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