X-ray diffraction study of bamboo fibers treated with NaOH |
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Authors: | Yanping Liu Hong Hu |
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Institution: | (1) Institute of Textile & Clothing, The Hong Kong Polytechnic University, Hung Hom, Kowloon, Hong Kong, China;(2) College of Textiles, Donghua University, Shanghai, 201620, P. R. China |
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Abstract: | Bamboo fibers are a new kind of natural materials which have a big potential application in textile field due to some of their
particular properties. However, high crystallinity and orientation structure can result in some undesirable properties and
this will limit their further applications as textile materials. As a common used way, mercerization was adapted to treat
bamboo fibers in this work in order to improve their undesirable properties. X-ray diffraction (XRD) was used to characterize
their microstructure after treatment with NaOH. The amount of cellulose II and the crystallinity index based on the XRD results
were calculated for the evaluation of the effectiveness of the different treatment conditions, such as alkali concentration,
mercerization duration and temperature, as well as tension applied to the fibers during mercerization, on the transformation
degree of cellulose I to cellulose II and decrystallization of the mercerized bamboo fibers. It has been found that each condition
has different effects and that the greatest effectiveness of crystal lattice conversion and decrystallization could be achieved
with such mercerization condition: 16 % alkali concentration, 10 minutes of mercerization at 20 °C without tension applied
to the fibers. |
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Keywords: | Mercerization Bamboo fiber Cellulose Sodium hydroxide X-ray diffraction Crystallinity |
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