| 除草剂安全剂AD-67的合成与表征 |
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| 引用本文： | 叶非 张荣全. 除草剂安全剂AD-67的合成与表征[J]. 东北农业大学学报, 1998, 29(3): 296-300 |
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| 作者姓名： | 叶非 张荣全 |
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| 作者单位： | 东北农业大学 |
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| 摘 要： | 报道了以乙醇胺和环己酮脱水缩合得螺［４，５］－１－氧杂－４－氮杂癸烷，再经与二氯乙酰氯反应制得标题化合物，两步总收率５５３０％。产品用ＩＲ、１Ｈ－ＮＭＲ和元素分析进行表征。
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| 关 键 词： | AD-67，合成，表征 |
SYNTHESIS AND CHARACTERIZATION OF HERBICIDE SAFENER AD-67 |
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| Ye Fei,Zhang Rongquan,Li Dongmei. SYNTHESIS AND CHARACTERIZATION OF HERBICIDE SAFENER AD-67[J]. Journal of Northeast Agricultural University, 1998, 29(3): 296-300 |
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| Authors: | Ye Fei Zhang Rongquan Li Dongmei |
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| Abstract: | Ethanolamine reacted with cyclohexanone through condensation to prepare 1-oxa-4-azaspiro-4,5-decane, then acylation with dichloroacetyl chloride to synthesis the title compound. The overall yield of the two steps was 55.3%. The product was characterized by means of IR, 1 H-NMR and elemental analysis. |
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| Keywords: | AD-67 synthesis characterization |
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