| 40%毒死蜱可湿性粉剂在苹果及土壤中的残留与消解动态 |
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| 引用本文： | 刘 磊,邵 辉,李 娜,李 晶,李 辉,张玉婷,宋淑荣,郭永泽.40%毒死蜱可湿性粉剂在苹果及土壤中的残留与消解动态[J].天津农业科学,2014(5):71-73. |
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| 作者姓名： | 刘 磊 邵 辉 李 娜 李 晶 李 辉 张玉婷 宋淑荣 郭永泽 |
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| 作者单位： | 天津市农业质量标准与检测技术研究所,天津300381 |
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| 摘 要： | 为评价毒死蜱在苹果上使用的安全性,并建立其使用规范,对毒死蜱在苹果及其种植土壤中的残留及消解动态进行研究。样品经乙腈提取,液液分配后,用气相色谱仪FPD检测器测定,外标法定量。毒死蜱在苹果和土壤中半衰期分别为3.6~8.2 d、5.8~11.5 d;检测的苹果中的最终残留量为0.001~0.019 mg·kg-1,土壤中的最终残留量为0.001~0.005 mg·kg-1。
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| 关 键 词： | 毒死蜱 苹果 土壤 消解动态 农药残留 |
Residue and Degradation Dynamics of Chlorpyrifos 40 % Wettable Powder in Apple and Soil |
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| LIU Lei,SHAO Hui,LI Na,LI Jing,LI Hui,ZHANG Yu-ting,SONG Shu-rong,GUO Yong-ze.Residue and Degradation Dynamics of Chlorpyrifos 40 % Wettable Powder in Apple and Soil[J].Tianjin Agricultural Sciences,2014(5):71-73. |
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| Authors: | LIU Lei SHAO Hui LI Na LI Jing LI Hui ZHANG Yu-ting SONG Shu-rong GUO Yong-ze |
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| Institution: | (Research Institution of Agricultural Quality Standards and Testing Technology in Tianjin, Tianjin 300381, China) |
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| Abstract: | To evaluate the safety of Chlorpyrifos in apple and establish its use specification, residue and degradation dynamics of Chlorpyrifos were tested. Samples were extracted by acetonitrile, and analyzed by GC with FPD detector using external standard method. The half-life of Chlorpyrifos in apple and soil were 3.6 to 8.2 days and 5.8 to 11.5 days, respectively. Final residues of Chlorpyrifos in apple was 〈0.001-0.019 mg·kg-1, and 〈0.001-0.005 mg·kg-1 in soil. |
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| Keywords: | Chlorpyrifos apple soil degradation dynamics pesticide residue |
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