| 液相色谱-荧光法测定甲氨基阿维菌素苯甲酸盐在甘蓝和土壤中的残留 |
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| 引用本文： | 孙明娜,万宇,朱传明,段劲生,王梅,高同春,花日茂. 液相色谱-荧光法测定甲氨基阿维菌素苯甲酸盐在甘蓝和土壤中的残留[J]. 安徽农业科学, 2008, 36(18) |
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| 作者姓名： | 孙明娜 万宇 朱传明 段劲生 王梅 高同春 花日茂 |
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| 作者单位： | 安徽农业大学资源与环境学院,安徽合肥,230036;安徽省农业科学院植保所,安徽合肥,230031;安徽省农产品品质改良重点实验室,安徽合肥,230031;安徽省化工研究院,安徽合肥,230031;安徽省农业科学院植保所,安徽合肥,230031;安徽省农产品品质改良重点实验室,安徽合肥,230031;安徽农业大学资源与环境学院,安徽合肥,230036 |
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| 摘 要： | 利用反相高效液相色谱-荧光法分析测定土壤、甘蓝中甲氨基阿维菌素苯甲酸盐的残留量。甲氨基阿维菌素苯甲酸盐在10~500 ng/ml(r=0.999 6)范围内峰面积与进样量呈良好的线性关系,平均回收率甘蓝为95.61%,变异系数为0.4%;土壤中为81.4%,变异系数为4.9%。该法操作简便、快速,回收率较高。
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| 关 键 词： | 高效液相色谱 甲氨基阿维菌素苯甲酸盐 残留检测 |
Determination of the Residual of Emamectin Benzoate in Cabbage and Soil with HPLC Fluorescence Detection |
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| SUN Ming-na et al. Determination of the Residual of Emamectin Benzoate in Cabbage and Soil with HPLC Fluorescence Detection[J]. Journal of Anhui Agricultural Sciences, 2008, 36(18) |
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| Authors: | SUN Ming-na et al |
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| Abstract: | The high performance liquid chromatographic method with fluorescence detection was used for the determination of emamectin benzoate in cabbage and soil.Good linearity of emamectin benzoate was obtained over the ranges of 10～500 ng/ml(r=0.999 6).The average recovery rate of emamectin benzoate was 95.61%(RSD 0.4%) in cabbage and 81.4%(RSD 4.9%) in soil.This method was simple,quick and the recovery rate was better. |
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| Keywords: | High performance liquid chromatography Emamectin benzoate Residue determination |
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