| 白黄散胶囊质量标准的研究 |
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| 引用本文： | 仇雅静. 白黄散胶囊质量标准的研究[J]. 中国兽药杂志, 2010, 44(5): 38-41 |
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| 作者姓名： | 仇雅静 |
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| 作者单位： | 1. 江苏省泰州药品检验所,泰州,225300
2. 江苏畜牧兽医职业技术学院,泰州,225300 |
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| 摘 要： | 建立了白黄散胶囊的质量标准。用薄层色谱法鉴别白头翁、黄芪、黄连、黄柏、山楂、乌梅、诃子,以高效液相色谱法测定盐酸小檗碱的含量。结果薄层色谱图斑点清晰,阴性对照无干扰,盐酸小檗碱在9.91～148.65μg/mL范围内与峰面积线性关系良好,加样回收率为97.70%,RSD为1.30%。所建立的方法简便、准确、重现性好,可用于白黄散胶囊的质量控制。
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| 关 键 词： | 白黄散胶囊 薄层色谱法 盐酸小檗碱 高效液相色谱法 |
| 收稿时间： | 2010-02-25 |
| 修稿时间： | 2010-04-14 |
Study of Quality Standard of Baihuangsan Capsules |
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| QIU Ya-jing,YU Jie,YE Hui,CHEN Xiao-peng. Study of Quality Standard of Baihuangsan Capsules[J]. Chinese Journal of Veterinary Drug, 2010, 44(5): 38-41 |
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| Authors: | QIU Ya-jing YU Jie YE Hui CHEN Xiao-peng |
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| Affiliation: | QIU Ya-jing1,YU Jie2,YE Hui1,CHEN Xiao-peng1 (1.Taizhou Institute for Drug Control,Taizhou 225300,2.Jiangsu Animal Husb,ry &Veterinary College,China) |
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| Abstract: | A quality standards was established for Baihuangsan Capsules.Radix pulsatillae,Radix astragali,Rhizoma coptidis,Cortex phellodendri,Fructus crataegi,Fructus mume and Fructus chebulae were identified by TLC.The content of berberine hydrochloride was determined by HPLC.The results of TLC spots were clear and negative comparison with no disturbance.The quantitative evaluation of berberine hydrochloride had the linear range of 9.91～148.65 μg/mL,the average recovery was 99.70%（RSD=1.30%）.This method is simple and accurate with high specificity and good repeatability.It is suitable for quality control of Baihuangsan Capsules. |
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| Keywords: | Baihuangsan capsules TLC berberine hydrochloride HPLC |
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