| 含嘧啶氧基和一氟甲氧基的吡唑邻甲酰氨基苯甲酰胺的合成及杀虫活性 |
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| 引用本文： | 曹敏,刘钢,窦花妮,邢家华,孔小林,姚巍,张秋颖,薛瑞,王农,姬文娟.含嘧啶氧基和一氟甲氧基的吡唑邻甲酰氨基苯甲酰胺的合成及杀虫活性[J].农药学学报,2012,14(1):99-102. |
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| 作者姓名： | 曹敏 刘钢 窦花妮 邢家华 孔小林 姚巍 张秋颖 薛瑞 王农 姬文娟 |
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| 作者单位： | 1.兰州交通大学 化学与生物工程学院, 兰州 730070 |
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| 基金项目： | 浙江省科技厅省属科研院所专项(2010F20009). |
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| 摘 要： | 以取代邻氨基苯甲酸和取代吡啶基吡唑羧酸为原料,合成了10个结构新颖的含嘧啶基和一氟甲氧基的吡唑邻甲酰氨基苯甲酰胺类化合物,其结构通过1H NMR和MS表征。盆栽法试验表明,在500 mg/L 质量浓度下,部分化合物对小菜蛾 Plutella xylostella 和苜蓿蚜 Aphis medicaginis的相对防效达100%。
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| 关 键 词： | 邻甲酰氨基苯甲酰胺 嘧啶 吡唑 合成 杀虫活性 |
| 收稿时间： | 7/5/2011 12:00:00 AM |
| 修稿时间： | 2011/11/16 0:00:00 |
Synthesis and insecticidal activity of pyridin- or fluoromethoxy- pyrazol-pyrimidine-carboxamides |
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| CAO Min,LIU Gang,DOU Huani,XING Jiahu,KONG Xiaolin,YAO Wei,ZHANG Qiuying,XUE Rui,WANG Nong and JI Wenjuan.Synthesis and insecticidal activity of pyridin- or fluoromethoxy- pyrazol-pyrimidine-carboxamides[J].Chinese Journal of Pesticide Science,2012,14(1):99-102. |
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| Authors: | CAO Min LIU Gang DOU Huani XING Jiahu KONG Xiaolin YAO Wei ZHANG Qiuying XUE Rui WANG Nong and JI Wenjuan |
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| Institution: | 1.College of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, China2.Zhejiang Base of National Southern Pesticide Research Centre, Zhejiang Research Institute of Chemical Industry, Hangzhou 310023, China |
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| Abstract: | Ten novel title compounds were synthesized from corresponding 2-aminobenzoic acid and pyridin- pyrazol-5-carboxylic acid.The structures of the compounds were confirmed by 1H NMR and MS.The results of biological tests indicated that some of the title compounds showed 100% inhibitory activity against diamond back moth and aphis craccivora at 500 mg/L. |
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| Keywords: | anthranilic diamides pyrimidine pyrazole synthesis insecticidal activity |
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