红参中非挥发脂溶性成分含量测定 |
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引用本文: | 杨会芳,李德坤,周大铮,杨悦武,叶正良,张勉,鞠爱春.红参中非挥发脂溶性成分含量测定[J].人参研究,2014(1):6-8. |
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作者姓名: | 杨会芳 李德坤 周大铮 杨悦武 叶正良 张勉 鞠爱春 |
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作者单位: | [1]中国药科大学中药学院,南京211198 [2] 天津天士力之骄药业有限公司,天津300402 |
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基金项目: | 天津市科技重大专项“重大新药创制”,项目编号:2013ZX09402202. |
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摘 要: | 目的测定红参中非挥发脂溶性物质的含量。方法:以提取溶剂用量、提取时间和提取次数为考察对象设计正交试验,采用回流法提取红参中的非挥发脂溶性成分。结果正交试验最佳优化方案为A3B2C3,即12倍量提取溶剂,提取4次,每次2小时。结论经验证,此法普遍适用于各批红参药材,为红参非挥发脂溶性成分的含量测定提供一个参考。
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关 键 词: | 红参 非挥发脂溶性物质 含量测定 |
Determination of non-volatile fat-soluble component content in Ginseng Radix |
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Authors: | YANG Huifang LI Dekun ZHOU Dazheng YANG Yuewuz YE Zhengliang ZHANG Mian JU Aichun |
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Institution: | 1. China Pharmaceutical University, Nanjing 211198, China; 2. Tianjin Tasly Pride Pharmaceutical Co., Ltd., Tianjin 300402, China) |
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Abstract: | Objective: the non-volatile fat-soluble component content in Ginseng Radix were determine. Method: refluxing extraction was adopted to design the orthogonal experiment, extraction solvent dosage, extraction time and extraction times as the investigation object extract the fat-soluble components in the Ginseng Radix. Results: Orthogonal test the best optimization scheme for A3B2C3, i.e., 12 times the amount of extraction solvent, extraction four times, each time 2 hours. Conclusion verified that this method is generally applied to each batch of Ginseng Radix, for removal and test of Ginseng Radix non-volatile fat-soluble components to provide a reference. |
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Keywords: | Ginseng Radix non-volatile fat-soluble component Content determination |
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