HPLC荧光检测鱼肉中孔雀石绿残留量的不确定度 |
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引用本文: | 曹向英,沈林辉,孙文梅,朱骏,唐丹丹,金立. HPLC荧光检测鱼肉中孔雀石绿残留量的不确定度[J]. 四川畜牧兽医, 2014, 0(4): 32-34 |
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作者姓名: | 曹向英 沈林辉 孙文梅 朱骏 唐丹丹 金立 |
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作者单位: | 上海市松江区食用农产品安全监督检测中心; |
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摘 要: | 通过数学建模,对GB/T20361-2006 HPLC法荧光检测鱼肉中孔雀石绿残留量的不确定度进行分析。结果表明,合成标准不确定度U(X)=0.048,测量鱼肉中孔雀石绿残留量的不确定度为(2.00±0.19)μg/kg。
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关 键 词: | 高效液相色谱 不确定度 荧光检测 孔雀石绿 |
HPLC with Fluorescence Detecting the Uncertainty of Malachite Green Residues in Fish |
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Affiliation: | CAO Xiang-ying, SHEN Lin-hui, SUN Wen-mei, et al. (Songjiang District of Edible Agricultural Products Safety Supervision and Inspection Center, Shanghai Songjiang 201611, China) |
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Abstract: | The purpose of this study was to analyze the determination uncertainty of the mala- chite green residue in fish which was determined by establishing HPLC with fluorescence detection method, according to GB/T 20361-2006 based on the mean of rmathematical modeling. The result showed that the combined standard uncertainty was 0.048, and the uncertainty of malachite green residues in fish was (2.00±0.19)μg/kg. |
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Keywords: | HPLC Uncertainty Fluorescence detection Malachite green |
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