| 混合酸浸出-火焰原子吸收法快速检测虾蛄中的镉元素 |
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| 引用本文： | 刘琴,钟志,祝银,王范盛. 混合酸浸出-火焰原子吸收法快速检测虾蛄中的镉元素[J]. 农业科学与技术, 2016, 0(12): 2732-2733 |
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| 作者姓名： | 刘琴 钟志 祝银 王范盛 |
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| 作者单位： | 1. 浙江省海洋水产研究所，浙江舟山 316021; 浙江省海洋渔业资源可持续利用技术研究重点实验室，浙江舟山 316021;2. 浙江省海洋水产研究所,浙江舟山,316021 |
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| 基金项目： | 浙江省科技计划项目(2015C32001)；浙江省省科技厅院所专项(2016F30021)；国家自然科学基金(21407127)。Supported by Science and Technology Planning Project of Zhejiang Province(2015C32001)，Special Fund for Research lnstitutes from Science and Technology Department of Zhejiang Province(2016F30021)，Natural Science Foundation of China(21407127) |
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| 摘 要： | [目的]寻找快速检测虾蛄中镉元素的方法。[方法]研究了混合酸浸出-火焰原子吸收法快速测定虾蛄中镉的方法，通过硝酸和硫酸5：1混合消解浸出镉，选择火焰原子吸收光谱仪测定样品中的镉含量。[结果]镉含量在1.0～2.0 mg/kg，加标回收率在86%～109%，RSD 0～6%。[结论]该方法快速简易，操作性强，重现性好，结果准确。
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| 关 键 词： | 虾蛄 火焰原子吸收 酸浸 镉 |
Rapid Determination of Cd in Squilla by Mixed Acid Leaching-flame Atomic Absorption Method |
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| Abstract: | Objective] This study was conducted to find a method for rapid determi-nation of Cd in squil a. [Method] Cd in squil a was determined by mixed acid leach-ing-flame atomic absorption method by digesting samples with HNO3-HSO4 (5:1) and determining Cd in the samples by a flame atomic absorption spectrophotometer. [Results] The Cd contents in squil a were 1.0-2.0 mg/kg, and the recoveries of Cd were 86%-109%, and the relative standard deviations were 0-6%. [Conclusion] The method is simple and rapid with strong operability, good reproducibility and high ac-curacy. |
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| Keywords: | Squilla Flame atomic absorption Mixed acid leaching Cd |
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