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Preparation and Characterization of Microcrystalline Cellulose from Sacred Bali Bamboo as Reinforcing Filler in Seaweed-based Composite Film
Authors:H. P. S. Abdul Khalil  Tze Kiat Lai  Ying Ying Tye  M. T. Paridah  M. R. Nurul Fazita  A. A. Azniwati  Rudi Dungani  Samsul Rizal
Affiliation:1.School of Industrial Technology,Universiti Sains Malaysia,Penang,Malaysia;2.Institute of Tropical Forestry and Forest Products (INTROP),Universiti Putra Malaysia,Serdang, Selangor,Malaysia;3.School of Life Sciences and Technology, Gandung Labtex XI,Institut Teknologi Bandung,Bandung,Indonesia;4.Mechanical Engineering Department,Syiah Kuala University,Banda Acheh,Indonesia
Abstract:Microcrystalline cellulose (MCC) isolated from cheap, fast-growing and abundant accessible Sacred Bali bamboo (Schizostachyum brachycladum) was utilized as reinforcement material in the seaweed-based composite film. Isolation of MCC was carried out by using a combination of pulping, bleaching and acid hydrolysis process. This study emphasized on the feasibility of MCC production from Sacred Bali bamboo by studying its properties using X-ray diffraction (XRD), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA). The commercial-MCC (CMCC) was used as reference material. Results showed that the production yield, moisture content (MC) and fiber length of bamboo-MCC (BMCC) were 83.37±1.48 %, 4.50±0.5 %, and 0.47±0.02 mm, respectively. According to the chemical analysis by FTIR, both lignin and hemicellulose were completely removed from BMCC, and thus, improved the crystallinity (78 %) and thermal stability (≈325 °C) of BMCC. This study also revealed that MCC produced from Sacred Bali bamboo demonstrated strong mechanical reinforcement effect in the seaweed-based film. Hence, Sacred Bali bamboo-MCC could be used as reinforcement material in the polymer.
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