| 饲料中总砷测定方法的研究 |
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| 引用本文： | 李胜,李宏,杨汉卿. 饲料中总砷测定方法的研究[J]. 中国农业科技导报, 2008, 10(Z2): 5-9 |
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| 作者姓名： | 李胜 李宏 杨汉卿 |
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| 作者单位： | 农业部饲料质量监督检验测试中心（西安） |
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| 摘 要： | 研究分析了饲料中总砷测定的不同前处理方法与检测方法对总砷测定结果的影响。结果表明,混合酸消解法对配合饲料、浓缩饲料、预混饲料中总砷的测定重复性好,精确度高;氢化物发生原子荧光光谱法测定饲料中总砷灵敏度高、回收率高、检测限低(3.6×10-11g/mL),同时具有污染小、操作简单便捷等优点。
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| 关 键 词： | 总砷 混合酸消解法处理 原子荧光光谱法 |
Determination of Total Arsenic in Feed |
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| LI Sheng,LI Hong,YANG Han-qing. Determination of Total Arsenic in Feed[J]. Journal of Agricultural Science and Technology, 2008, 10(Z2): 5-9 |
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| Authors: | LI Sheng LI Hong YANG Han-qing |
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| Affiliation: | Feed Quality Supervision and Testing Center（Xi an）|Ministy of Agriculture|Xi an 710016|China |
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| Abstract: | The different pretreatment methods and measure methods of total arsenic in feed were studied.The result showed that mixed acid digestion method had better reproducibility and accuracy when testing total arsenic in compoand feed,concentrated feed and premix digestion.Atomic fluorescence spectrometry of hydrid reaction method had high sensitivity,high reclaim ratio and low detection limit(3.6×10-11 g/mL) with advantages of lower pollution and simple operation. |
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| Keywords: | total arsenic mixed acid digestion method atomic fluorescence spectrometry method |
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