| 高效液相色谱-质谱联用技术测定毛榛中的紫杉醇含量 |
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| 引用本文： | 罗凡,费学谦,汤富彬,李辛雷.高效液相色谱-质谱联用技术测定毛榛中的紫杉醇含量[J].林业科学研究,2011,24(6):779-783. |
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| 作者姓名： | 罗凡 费学谦 汤富彬 李辛雷 |
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| 作者单位： | 中国林业科学研究院亚热带林业研究所,浙江富阳,311400 |
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| 基金项目： | 中国林科院亚热带林业研究所所长基金(RISF6921);浙江省省院合作林业科技项目(2007SY10) |
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| 摘 要： | Established method by reverse phase HPLC and electrospray ionization mass spectrometry (HPLC-ESI-MS) analysis and hazelnut extract trace of taxol. Through the research, seven mass spectrum characteristics of taxol compounds were contested, and the taxanes database was initially established. It was found that the paciltaxel contents were 23.65 μg·mL-1 and 4.09 μg·mL-1 in leaves and stems respectively. The paciltaxel contents in different parts of hazelnut was slightly different, which were 0.61, 0.23 and 0.35 μg·mL-1 in hazel branch, leaf and leather. With these data it can quickly identify the known paclitaxel compounds in hazelnut extract, and can perform the unknown structure analysis to certain degrees. This analysis method is confirmed sensitive, reliable and fast.
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| 关 键 词： | 高效液相色谱-质谱 紫杉醇 毛榛 |
| 收稿时间： | 2011/3/21 0:00:00 |
Simultaneous Determination of Paclitaxel in Hazelnut by HPLC-MS/MS |
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| LUO Fan,FEI Xue-qian,TANG Fu-bin and LI Xin-lei.Simultaneous Determination of Paclitaxel in Hazelnut by HPLC-MS/MS[J].Forest Research,2011,24(6):779-783. |
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| Authors: | LUO Fan FEI Xue-qian TANG Fu-bin and LI Xin-lei |
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| Institution: | Research Institute of Subtropical Forestry, Chinese Academy of Forestry, Fuyang 311400, Zhejiang, China;Research Institute of Subtropical Forestry, Chinese Academy of Forestry, Fuyang 311400, Zhejiang, China;Research Institute of Subtropical Forestry, Chinese Academy of Forestry, Fuyang 311400, Zhejiang, China;Research Institute of Subtropical Forestry, Chinese Academy of Forestry, Fuyang 311400, Zhejiang, China |
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| Abstract: | |
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| Keywords: | HPLC-MS/MS paciltaxel hazelnut |
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