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微波法制备玉米穗轴活性炭及其应用研究
引用本文:蒋莉,马飞,李想,叶招莲. 微波法制备玉米穗轴活性炭及其应用研究[J]. 新疆农业大学学报, 2010, 33(2): 158-161
作者姓名:蒋莉  马飞  李想  叶招莲
作者单位:1. 江苏技术师范学院,化学化工学院,常州,213001
2. 江苏技术师范学院,化学化工学院,常州,213001;河海大学,水利水电工程学院,南京,210098
3. 东南大学化学化工学院,南京,210096
基金项目:江苏省自然科学基金项目 
摘    要:以微波为热源,以NaOH为活化剂采用化学活化法制备玉米穗轴活性炭,结果表明,微波功率462W、NaOH浓度15%、液固比3.5:1、辐照时间5min时活性炭的碘值为1095.45mg/g,平均产率为20.32%。应用其处理废水的结果显示,对COD为229.33mg/L废水投加7.5%活性炭时,经70min吸附后对COD的去除率为78.28%,接近商品活性炭对COD的去除率(83.14%),但其具有来源广泛、价格低廉的特点,可以预见还是具有市场竞争力的。

关 键 词:玉米穗轴  活性炭  微波法  NaOH

Preparation of Activated Carbon from Corn Cob by Microwave Heating and Its Application
JIANG Li,MA Fei,LI Xiang,YE Zhao-lian. Preparation of Activated Carbon from Corn Cob by Microwave Heating and Its Application[J]. Journal of Xinjiang Agricultural University, 2010, 33(2): 158-161
Authors:JIANG Li  MA Fei  LI Xiang  YE Zhao-lian
Affiliation:JIANG Li1,MA Fei1,2,LI Xiang3,YE Zhao-lian1(1.School of Chemistry & Chemical Engineering,Jiangsu Teachers University of Technology,Changzhou 213001,China,2.The College of Water Conservancy , Hydropower Engineering,Hohai University,Nanjing 210098,3.School of Chemistry & Chemical Engineering,Southeast University,Nanjing 210096,China)
Abstract:Microwave irradiation was used as a heat source in the preparation of activated carbon (AC) from corn cob by NaOH chemical activation. By optimizing reaction conditions of microwave power of 462W,NaOH solution concentration of 15% ,ratio of liquidtosolid 3.5 : 1 and the microwave radiation time of 5 rain,maximum odine number of 1 095.45 mg/g were achieved. Furthermore, the prepared AC was applied to wastewater treatment, and results showed that,when 7.5 % mass fraction addition of AC were applied,the COD of wasterwater was decreased from initial value of 229.33 to 50.40 mg/L (removal rate of 78.28%) after 70 min adsorption,suggesting removal rate was similar to commercial AC. Undoubtedly, due to wide source of raw materials and cheap price,it can foresee that there will still be market competive power in the future.
Keywords:NaOH
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