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| 土壤中POPs检测方法参数的优化 | |
| 引用本文： | 凌建刚,王方盛,朱优峰,陈 国,康孟利,陈海燕,吕 燕,俞静芬 钱天寿,王美英,赵 健,朱 勇.土壤中POPs检测方法参数的优化[J].中国农学通报,2008,24(7):430-435. |
| 作者姓名： | 凌建刚 王方盛 朱优峰 陈 国 康孟利 陈海燕 吕 燕 俞静芬 钱天寿 王美英 赵 健 朱 勇 |
| 作者单位： | 1. 宁波市农科院农产品加工研究所,浙江宁波,315040 2. 宁波市农业局科教处,浙江宁波,315012 3. 浙江大学环境工程系,浙江杭州,310029 4. 华中农业大学,湖北武汉,430070 5. 宁波市农产品质量检测中心,浙江宁波,315040 6. 浙江宁海县农产品监测中心,浙江宁海,315600 |
| 基金项目： | 浙江省宁波市科技攻关项目 , 浙江省宁波市农业科技成果转化基金 |
| 摘 要： | 研究了环境土壤中部分毒害性有机污染物的多残留监测确证技术，采用符合实际的采样方案，应用超声提取、固相萃取前处理及净化手段，充分发挥气相色谱（GC）双柱双检测器和气相色谱-质谱联用（GC-MS）选择离子监测（SIM）优势互补技术，建立了环境土壤中艾氏剂等10种持久性有机污染物多残留检测确证方法。充分挖掘GC和MS的互补优化技术，通过标准添加和对实际样品的监测，证明方法具有前处理简洁、速度快、定量检测和定性确证结合、适合批量等优点。 |
| 关 键 词： | 农学研究 农学研究 哲学基础 方法论 |
| 收稿时间： | 2008/3/27 0:00:00 |
| 修稿时间： | 2008/5/12 0:00:00 |
Parameter Optimization of Determination In soil POPs |
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| Ling Jiangang,Wang Fangsheng,Zhu Youfeng,Chen Guo,Kang Mengli,Chen Haiyan,Lu Yan,Yu Jingfen,Qian Tianshou,Wang Meiying,Zhao Jian,Zhu Yong.Parameter Optimization of Determination In soil POPs[J].Chinese Agricultural Science Bulletin,2008,24(7):430-435. | |
| Authors: | Ling Jiangang Wang Fangsheng Zhu Youfeng Chen Guo Kang Mengli Chen Haiyan Lu Yan Yu Jingfen Qian Tianshou Wang Meiying Zhao Jian Zhu Yong |
| Institution: | 1Ningpo Institute of Agricultural Sciences Agricultural products processing Research institute, Ningbo, 315040; 2 Ningpo Bureau of agriculture science and technology education place, Zhejiang Ningbo 315012; 3Zhejiang University environment engineering department, Hangzhou, 310029; 4Central China Agricultural college, 430070, Hubei Wuhan; 5Ningpo agricultural product quality detection center, Ningbo, 315040; 6Zhejiang Ninghai County agricultural product monitor center, Ninghai, 315600 |
| Abstract: | This item studied the determination and conformation of the toxic organic pollutants in the environment. The samples were extracted by ultrasonication and further purified by solid phase extraction. Quantitative analysis was carried out using gas chromatograph (GC) equipped with double columns and coupled to a MSD operated in the selected ion-monitoring mode (SIM), respectively, to confirm the identification of compounds. Detection methods of 10 kinds of organic pollutants in soil were established. For quality assurance and quality control according to U.S. |
| Keywords: | Environment Organic Pollutants Determination GC-MS |
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