| QuEChERS_GPC_GC_MS快速测定蔬菜中24种农药残留 |
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| 引用本文： | 吴春梅,程雪梅,李 亮,叶瑜霏,张少丰,陈健航. QuEChERS_GPC_GC_MS快速测定蔬菜中24种农药残留[J]. 热带作物学报, 2012, 32(2): 52-56 |
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| 作者姓名： | 吴春梅 程雪梅 李 亮 叶瑜霏 张少丰 陈健航 |
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| 作者单位： | 东莞市农产品质量安全监督检测所 广东东莞 523086;东莞市农产品质量安全监督检测所 广东东莞 523086;东莞市农产品质量安全监督检测所 广东东莞 523088;东莞市农产品质量安全监督检测所 广东东莞 523086;东莞市农产品质量安全监督检测所 广东东莞 523086;东莞市农产品质量安全监督检测所 广东东莞 523086 |
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| 摘 要： | 采用QuEChERS前处理方法和在线凝胶渗透色谱-气相色谱质谱联用仪(gel permeation chromatography-gas chromatography/mass spectrometry，GPC-GC/MS)快速测定蔬菜中24种多农药残留。样品经乙腈提取，净化采用分散固相萃取的方式，加标浓度为0.1 mg/kg，油麦菜样品中的24种农药回收率大部分在70%～120%，24种农药的检出限范围在0.000 2～0.009 mg/kg，线性范围0.025～0.30 mg/L，相对标准偏差在1.41%～10.05%，满足农药多残留的分析要求。实验表明，QuEChERS方法提取和净化使样品前处理更为简单、方便、快速，GPC-GC/MS系统中的GPC柱弥补了QuEChERS方法去除干扰物不彻底的问题，能更准确地检测出蔬菜中多农药残留，检测灵敏度高，重现性好。
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| 关 键 词： | 在线凝胶渗透色谱 ；气相色谱-质谱 ；多农药残留 ；QuEChERS |
Quick Determination of 24 Pesticide Residues in Vegetables with QuEChERS_GPC_GC_MS |
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| Affiliation: | Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086;Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086;Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086;Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086;Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086;Dongguan Supervision and Test Institution of Agricultural Product Quality and Safety, Dongguan, Guangdong 523086 |
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| Abstract: | |
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| Keywords: | online gel permeation chromatography (GPC) gas chromatography/mass spectrometry (GC/MS) Multi-Pesticide Residues QuEChERS |
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