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蒸馏时间对丁香油化学成分的影响
引用本文:田玉红,黄琼,陈志燕,蒋宏霖,张祥民. 蒸馏时间对丁香油化学成分的影响[J]. 安徽农业科学, 2009, 37(30): 14542-14543
作者姓名:田玉红  黄琼  陈志燕  蒋宏霖  张祥民
作者单位:广西中烟工业有限责任公司技术中心,广西,柳州,545005;复旦大学化学系,上海,200433;广西工学院生物与化学工程系,广西,柳州,545006;广西工学院生物与化学工程系,广西,柳州,545006;广西中烟工业有限责任公司技术中心,广西,柳州,545005;复旦大学化学系,上海,200433
基金项目:广西教育厅科研项目资助,广西中烟工业有限责任公司科技创新项目 
摘    要:[目的]考察蒸馏时间对丁香油化学成分的影响。[方法]采用水蒸气蒸馏法提取不同蒸馏时段的精油馏分,通过气相色谱-质谱(GC-MS)映用分析鉴定其化学成分。[结果]不同蒸馏时段丁香油的主要化学成分为:丁香酚(85.574%~58.519%)、乙酸丁香酚酯(8.845%-30.584%)、β-石竹烯(1.758%-5.680%)、α-石竹烯(0.257%~1.005%)。[结论]蒸馏时间对丁香油的化学成分有较大影响,随着蒸馏时间的延长,丁香酚的含量逐渐降低,而乙酸丁香酚酯的含量逐渐升高。

关 键 词:丁香  精油  蒸馏时间  成分分析

Effects of Distillation Duration on the Chemical Composition of Essential Oil from Eugenia caryophyllata Thunb
TIAN Yu-hong et al. Effects of Distillation Duration on the Chemical Composition of Essential Oil from Eugenia caryophyllata Thunb[J]. Journal of Anhui Agricultural Sciences, 2009, 37(30): 14542-14543
Authors:TIAN Yu-hong et al
Affiliation:TIAN Yu-hong et al (Technology Centre of Guangxi Zhongyan Industrial Limited Liability Corporation,Liuzhou,Guangxi 545005)
Abstract:[Objective] The aim was to study effects of distillation duration on the chemical composition of essential oil from Eugenia caryophyllata Thunb.[Method] The essential oil fractions collected at different times during distillation were obtained through hydrodistillation and analyzed by gas chromatography-mass spectrometry(GC-MS) method.[Result] The main constituents in oils collected at different times during distillation were eugenol(85.574%-58.519%),eugenol acetate(8.845%-30.584%),β-caryophyllene(1.758%-5.680%) and α-caryophyllene(0.257%-1.005%).[Conclusion] The constituents of oil from E.caryophyllata Thunb varied obviously with the duration of distillation.The relative content of eugenol decreased with the distillation processing,while that of euganol acetate increased.
Keywords:Eugenia caryophyllata Thunb  Essential oil  Distillation duration  Component analysis  
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