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微波消解ICP-AES同时测定南美白对虾饲料中8种微量元素
引用本文:覃丽霞,林冠春,邓全道,许光,罗虎,刘建发,梁德荣. 微波消解ICP-AES同时测定南美白对虾饲料中8种微量元素[J]. 饲料工业, 2011, 32(20)
作者姓名:覃丽霞  林冠春  邓全道  许光  罗虎  刘建发  梁德荣
作者单位:1. 钦州出入境检验检疫局,助理工程师,535000,广西钦州
2. 中国检验认证集团广西有限公司钦州分公司
摘    要:采用HNO3-H2O2作消解液进行微波消解,用电感耦合等离子体发射光谱法(Inductively cou-pled plasma-atomic emission spectrometryI,CP-AES)同时测定南美白对虾饲料中的Fe、Zn、Se、Cu等8种微量元素。结果显示,本法灵敏度高,准确性好,各元素测定结果的相对标准偏差在0.524%~1.695%之间,加标回收率在93.2%~101.4%之间。试验发现,南美白对虾饲料中含有较丰富的微量元素,能促进南美白对虾的生长发育。

关 键 词:微波消解  电感耦合等离子体发射光谱法  南美白对虾饲料  微量元素

Determination of eight trace elements contents in penaeus vannamei feeds by microwave digestion ICP-AES
Qin Lixia,Lin Guanchun,Deng Quandao,Xu Guang,Luo Hu,Liu Jianfa,Liang Derong. Determination of eight trace elements contents in penaeus vannamei feeds by microwave digestion ICP-AES[J]. Feed Industry, 2011, 32(20)
Authors:Qin Lixia  Lin Guanchun  Deng Quandao  Xu Guang  Luo Hu  Liu Jianfa  Liang Derong
Affiliation:Qin Lixia,Lin Guanchun,Deng Quandao,Xu Guang,Luo Hu,Liu Jianfa,Liang Derong
Abstract:The contents of eight trace elements(Fe,Zn,Se,Cu,Mn,Ni,Co and Sr)in Penaeus vannamei feeds were determined by ICP-AES(Inductively coupled plasma-atomic emission spectrometry).The samples were digested by microwave with HNO3-H2O2 solution as reagent.The determination results showed the method was sensitive and accurate.The relative standard deviations(RSD,n=5) were in the range of 0.524%~1.695%,and the recoveries were in the range of 93.2%~101.4%.There are abundant trace elements in Penaeus vannamei feeds,which could promote the growth of Penaeus vannamei.
Keywords:microwave digestion  inductively coupled plasma-atomic emission spectrometry  penaeus vannamei feeds  trace element  
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