| 3-硝基苯甲醛与硫代巴比妥酸固相反应的研究 |
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| 引用本文： | 王春,李贵深,李敬慈,张英群. 3-硝基苯甲醛与硫代巴比妥酸固相反应的研究[J]. 河北农业大学学报, 2002, 25(4): 126-127,133 |
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| 作者姓名： | 王春 李贵深 李敬慈 张英群 |
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| 作者单位： | 河北农业大学,理学院,河北,保定,071001 |
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| 摘 要： | 研究了3－硝基民硫代巴比妥酸固相反应，选择了反应的最佳条件。该反应操作简便，产品易提纯，反应收率高。产物结构经^1H NMR、^13C NMR、IR和UV确证。
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| 关 键 词： | 3－硝基苯甲醛 硫代巴比妥酸 5－[（3－硝基）苯亚甲基]硫代巴比妥酸 固相反应 反应条件 溶解性能 光谱特性 绿色合成 |
| 文章编号： | 1000-1573(2002)04-0126-02 |
Study of the solid state condensation reaction between 3-nitrobenzaldehyde and thiobarbituric acid |
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| WANG Chun,LI Gui-shen,LI Jing-ci,ZHANG Ying-qun. Study of the solid state condensation reaction between 3-nitrobenzaldehyde and thiobarbituric acid[J]. Journal of Agricultural University of Hebei, 2002, 25(4): 126-127,133 |
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| Authors: | WANG Chun LI Gui-shen LI Jing-ci ZHANG Ying-qun |
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| Abstract: | The solid state reaction of 3-nitrobenzaldehyde and 2-thiobarbituric acid was carried out.And the optimal operation conditions were obtained. And the structure of the product were identified by 1H NMR, 13C NMR,IR and UV. |
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| Keywords: | nitrobenzaldehyde thiobarbituric acid 5-[(3-nitro)arylidene]thiobarbituric acid solid state synthesis |
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